[3-[[(1,1-dimethylethyloxycarbonyl)-methyl]amino]propyl]carbamic acid phenylmethyl ester

Base Information

• Chemical Name: [3-[[(1,1-dimethylethyloxycarbonyl)-methyl]amino]propyl]carbamic acid phenylmethyl ester
• CAS No.: 144912-88-9
• Molecular Formula: C₁₇H₂₆N₂O₄
• Molecular Weight: 322.404

Synonyms:[3-[[(1,1-dimethylethyloxycarbonyl)-methyl]amino]propyl]carbamic acid phenylmethyl ester

Chemical Property of [3-[[(1,1-dimethylethyloxycarbonyl)-methyl]amino]propyl]carbamic acid phenylmethyl ester

Chemical Property:

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Technology Process of [3-[[(1,1-dimethylethyloxycarbonyl)-methyl]amino]propyl]carbamic acid phenylmethyl ester

There total 2 articles about [3-[[(1,1-dimethylethyloxycarbonyl)-methyl]amino]propyl]carbamic acid phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

bromoacetic acid tert-butyl ester (5292-43-3) + N-benzyloxycarbonyl-1,3-diaminopropane (46460-73-5) → 8,9-dioxo-2,6-diazabicyclo[5.2.0]non-1(7)-ene-2-acetic acid + [3-[[(1,1-dimethylethyloxycarbonyl)-methyl]amino]propyl]carbamic acid phenylmethyl ester (144912-88-9)

Guidance literature:

With sodium hydroxide; N-ethyl-N,N-diisopropylamine; In N-methyl-acetamide; dichloromethane;

Reference yield: 82.0%

bromoacetic acid tert-butyl ester (5292-43-3) + N-benzyloxycarbonyl-1,3-diaminopropane (46460-73-5) → [3-[[(1,1-dimethylethyloxycarbonyl)-methyl]amino]propyl]carbamic acid phenylmethyl ester (144912-88-9)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 10 - 20 ℃;

DOI:10.1021/jm970504g

Reference yield: 91.0%

3,4-diethoxy-3-cyclobuten-1,2-dione (5231-87-8) + [3-[[(1,1-dimethylethyloxycarbonyl)-methyl]amino]propyl]carbamic acid phenylmethyl ester (144912-88-9) → [3-[[(1,1-dimethylethyloxycarbonyl)methyl]-(2-ethoxy-3,4-dioxo-1-cyclobuten-1-yl)amino]-propyl]carbamic acid phenylmethyl ester (144912-89-0)

Guidance literature:

In ethanol; for 3.5h;

DOI:10.1021/jm970504g

upstream raw materials:

bromoacetic acid tert-butyl ester

N-benzyloxycarbonyl-1,3-diaminopropane

Downstream raw materials:

[3-[[(1,1-dimethylethyloxycarbonyl)methyl]-(2-ethoxy-3,4-dioxo-1-cyclobuten-1-yl)amino]-propyl]carbamic acid phenylmethyl ester

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