Technology Process of C19H23NO6S
There total 8 articles about C19H23NO6S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
iron; acetic acid;
In
methanol;
at 60 - 80 ℃;
for 3h;
DOI:10.1039/c3ob27220f
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium tert-butylate / tetrahydrofuran / 9 h / 0 - 20 °C
2: potassium tert-butylate / tetrahydrofuran / 2 h / Reflux
3: triethyl borane / dichloromethane; hexane / 8 h / -78 °C
4: oxone / tetrahydrofuran; methanol / 24 h / 20 °C
5: acetic acid; iron / methanol / 3 h / 60 - 80 °C
With
triethyl borane; oxone; potassium tert-butylate; iron; acetic acid;
In
tetrahydrofuran; methanol; hexane; dichloromethane;
DOI:10.1039/c3ob27220f
- Guidance literature:
-
Multi-step reaction with 5 steps
1: dibenzoyl peroxide; N-Bromosuccinimide / tetrachloromethane / 18 h / Reflux
2: thiourea / water / 2 h / Reflux
3: triethyl borane / dichloromethane; hexane / 8 h / -78 °C
4: oxone / tetrahydrofuran; methanol / 24 h / 20 °C
5: acetic acid; iron / methanol / 3 h / 60 - 80 °C
With
N-Bromosuccinimide; triethyl borane; oxone; iron; acetic acid; thiourea; dibenzoyl peroxide;
In
tetrahydrofuran; methanol; tetrachloromethane; hexane; dichloromethane; water;
DOI:10.1039/c3ob27220f