(S)-4-((3R,5R)-6-((2R,3S,6S)-6-allyl-3-methyltetrahydro-2H-pyran-2-yl)-5-methoxy-2-(4-methoxyphenyl)-2-methylhexan-3-yloxy)-6-(tert-butyldiphenylsilyloxy)hex-1-en-2-yl acetate

Base Information

Chemical Name:(S)-4-((3R,5R)-6-((2R,3S,6S)-6-allyl-3-methyltetrahydro-2H-pyran-2-yl)-5-methoxy-2-(4-methoxyphenyl)-2-methylhexan-3-yloxy)-6-(tert-butyldiphenylsilyloxy)hex-1-en-2-yl acetate
CAS No.:1001328-62-6
Molecular Formula:C₄₈H₆₈O₇Si
Molecular Weight:785.149
Hs Code.:

(S)-4-((3R,5R)-6-((2R,3S,6S)-6-allyl-3-methyltetrahydro-2H-pyran-2-yl)-5-methoxy-2-(4-methoxyphenyl)-2-methylhexan-3-yloxy)-6-(tert-butyldiphenylsilyloxy)hex-1-en-2-yl acetate

Synonyms:(S)-4-((3R,5R)-6-((2R,3S,6S)-6-allyl-3-methyltetrahydro-2H-pyran-2-yl)-5-methoxy-2-(4-methoxyphenyl)-2-methylhexan-3-yloxy)-6-(tert-butyldiphenylsilyloxy)hex-1-en-2-yl acetate

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Chemical Property of (S)-4-((3R,5R)-6-((2R,3S,6S)-6-allyl-3-methyltetrahydro-2H-pyran-2-yl)-5-methoxy-2-(4-methoxyphenyl)-2-methylhexan-3-yloxy)-6-(tert-butyldiphenylsilyloxy)hex-1-en-2-yl acetate

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Technology Process of (S)-4-((3R,5R)-6-((2R,3S,6S)-6-allyl-3-methyltetrahydro-2H-pyran-2-yl)-5-methoxy-2-(4-methoxyphenyl)-2-methylhexan-3-yloxy)-6-(tert-butyldiphenylsilyloxy)hex-1-en-2-yl acetate

There total 1 articles about (S)-4-((3R,5R)-6-((2R,3S,6S)-6-allyl-3-methyltetrahydro-2H-pyran-2-yl)-5-methoxy-2-(4-methoxyphenyl)-2-methylhexan-3-yloxy)-6-(tert-butyldiphenylsilyloxy)hex-1-en-2-yl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1001328-70-6
((R)-3-((3R,5R)-6-((2R,3S,6S)-6-allyl-3-methyltetrahydro-2H-pyran-2-yl)-5-methoxy-2-(4-methoxyphenyl)-2-methylhexan-3-yloxy)hex-5-ynyloxy)(tert-butyl)diphenylsilane

: 64-19-7,77671-22-8
acetic acid

: 1001328-62-6
(S)-4-((3R,5R)-6-((2R,3S,6S)-6-allyl-3-methyltetrahydro-2H-pyran-2-yl)-5-methoxy-2-(4-methoxyphenyl)-2-methylhexan-3-yloxy)-6-(tert-butyldiphenylsilyloxy)hex-1-en-2-yl acetate

Guidance literature:: With trifuran-2-yl-phosphane; sodium carbonate; [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; In toluene; at 80 ℃; for 36h;
DOI:10.1002/anie.200702999

Reference yield: 68.0%

: 1001328-62-6
(S)-4-((3R,5R)-6-((2R,3S,6S)-6-allyl-3-methyltetrahydro-2H-pyran-2-yl)-5-methoxy-2-(4-methoxyphenyl)-2-methylhexan-3-yloxy)-6-(tert-butyldiphenylsilyloxy)hex-1-en-2-yl acetate

: 1001328-63-7
(2R,6S)-2-((2S)-3-((2R,3S,6S)-6-allyl-3-methyltetrahydro-2H-pyran-2-yl)-2-methoxypropyl)-6-(2-(tert-butyldiphenylsilyloxy)ethyl)tetrahydropyran-4-one

Guidance literature:: With ammonium cerium(IV) nitrate; 4 A molecular sieve; sodium hydrogencarbonate; In 1,2-dichloro-ethane; acetonitrile; at 20 ℃; for 2h;
DOI:10.1002/anie.200702999