1,3-dibutyl-7-(4-hydroxyamino-benzenesulfonyl)-3,7-dihydro-purine-2,6-dione

Base Information

Chemical Name:1,3-dibutyl-7-(4-hydroxyamino-benzenesulfonyl)-3,7-dihydro-purine-2,6-dione
CAS No.:263552-95-0
Molecular Formula:C₁₉H₂₅N₅O₅S
Molecular Weight:435.504
Hs Code.:

Synonyms:1,3-dibutyl-7-(4-hydroxyamino-benzenesulfonyl)-3,7-dihydro-purine-2,6-dione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-dibutyl-7-(4-hydroxyamino-benzenesulfonyl)-3,7-dihydro-purine-2,6-dione

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Technology Process of 1,3-dibutyl-7-(4-hydroxyamino-benzenesulfonyl)-3,7-dihydro-purine-2,6-dione

There total 4 articles about 1,3-dibutyl-7-(4-hydroxyamino-benzenesulfonyl)-3,7-dihydro-purine-2,6-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1,3-dibutyl-7-(4-nitrobenzenesulfonyl)-3,7-dihydropurine-2,6-dione

: 263552-95-0
1,3-dibutyl-7-(4-hydroxyamino-benzenesulfonyl)-3,7-dihydro-purine-2,6-dione

Guidance literature:: With hydrogen; 10percent Pd/C; In ethyl acetate; at 23 ℃; for 8h; under 760.051 Torr;
DOI:10.1021/jm990558l

Reference yield: 85.0%

: 263552-95-0
1,3-dibutyl-7-(4-hydroxyamino-benzenesulfonyl)-3,7-dihydro-purine-2,6-dione

Guidance literature:

Reference yield:

: 2850-36-4
1,3-dibutylxanthine

: 263552-95-0
1,3-dibutyl-7-(4-hydroxyamino-benzenesulfonyl)-3,7-dihydro-purine-2,6-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / i-Pr₂NEt / CH₂Cl₂ / 24 h / 23 °C

2: 88 percent / H₂ / 10percent Pd/C / ethyl acetate / 8 h / 23 °C / 760.05 Torr

With hydrogen; N-ethyl-N,N-diisopropylamine; 10percent Pd/C; In dichloromethane; ethyl acetate; 1: sulfonylation / 2: Catalytic hydrogenation;
DOI:10.1021/jm990558l