N-succinimidyl-3-(4'-tert-butyldimethylsilyloxy-3',5'-bis(acetoxymethyl)phenyl)propionate

Base Information

Chemical Name:N-succinimidyl-3-(4'-tert-butyldimethylsilyloxy-3',5'-bis(acetoxymethyl)phenyl)propionate
CAS No.:372942-01-3
Molecular Formula:C₂₅H₃₅NO₉Si
Molecular Weight:521.64
Hs Code.:

Synonyms:N-succinimidyl-3-(4'-tert-butyldimethylsilyloxy-3',5'-bis(acetoxymethyl)phenyl)propionate

Suppliers and Price of N-succinimidyl-3-(4'-tert-butyldimethylsilyloxy-3',5'-bis(acetoxymethyl)phenyl)propionate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-succinimidyl-3-(4'-tert-butyldimethylsilyloxy-3',5'-bis(acetoxymethyl)phenyl)propionate

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Technology Process of N-succinimidyl-3-(4'-tert-butyldimethylsilyloxy-3',5'-bis(acetoxymethyl)phenyl)propionate

There total 2 articles about N-succinimidyl-3-(4'-tert-butyldimethylsilyloxy-3',5'-bis(acetoxymethyl)phenyl)propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 6066-82-6
1-hydroxy-pyrrolidine-2,5-dione

: 636604-49-4
3-[4'-tert-butyldimethylsilyloxy-3',5'-bis(acetoxymethyl)phenyl]propionic acid

: 372942-01-3
N-succinimidyl-3-(4'-tert-butyldimethylsilyloxy-3',5'-bis(acetoxymethyl)phenyl)propionate

Guidance literature:: With N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In N,N-dimethyl-formamide; at 4 ℃; for 20h;
DOI:10.1021/ja036943o

Reference yield:

: 636604-47-2
3-[4'-tert-butyldimethylsilyloxy-3',5'-bis(tert-butyldimethylsilyloxymethyl)]propionic acid

: 372942-01-3
N-succinimidyl-3-(4'-tert-butyldimethylsilyloxy-3',5'-bis(acetoxymethyl)phenyl)propionate

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / FeCl₃ / 0.5 h / 0 °C

2: 66 percent / 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide / dimethylformamide / 20 h / 4 °C

With iron(III) chloride; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In N,N-dimethyl-formamide;
DOI:10.1021/ja036943o