thexyldimethylsilyl {4,6-O-benzylidene-3-O-[(R)-(benzyloxycarbonyl)(cyclohexyl)methyl]-β-D-galactopyranosyl}-(1->3)-2-(acetylamino)-4,6-O-benzylidene-2-deoxy-β-D-galactopyranoside

Base Information

Chemical Name:thexyldimethylsilyl {4,6-O-benzylidene-3-O-[(R)-(benzyloxycarbonyl)(cyclohexyl)methyl]-β-D-galactopyranosyl}-(1->3)-2-(acetylamino)-4,6-O-benzylidene-2-deoxy-β-D-galactopyranoside
CAS No.:866890-23-5
Molecular Formula:C₅₁H₆₉NO₁₃Si
Molecular Weight:932.193
Hs Code.:

thexyldimethylsilyl {4,6-O-benzylidene-3-O-[(R)-(benzyloxycarbonyl)(cyclohexyl)methyl]-β-D-galactopyranosyl}-(1->3)-2-(acetylamino)-4,6-O-benzylidene-2-deoxy-β-D-galactopyranoside

Synonyms:thexyldimethylsilyl {4,6-O-benzylidene-3-O-[(R)-(benzyloxycarbonyl)(cyclohexyl)methyl]-β-D-galactopyranosyl}-(1->3)-2-(acetylamino)-4,6-O-benzylidene-2-deoxy-β-D-galactopyranoside

Suppliers and Price of thexyldimethylsilyl {4,6-O-benzylidene-3-O-[(R)-(benzyloxycarbonyl)(cyclohexyl)methyl]-β-D-galactopyranosyl}-(1->3)-2-(acetylamino)-4,6-O-benzylidene-2-deoxy-β-D-galactopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of thexyldimethylsilyl {4,6-O-benzylidene-3-O-[(R)-(benzyloxycarbonyl)(cyclohexyl)methyl]-β-D-galactopyranosyl}-(1->3)-2-(acetylamino)-4,6-O-benzylidene-2-deoxy-β-D-galactopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of thexyldimethylsilyl {4,6-O-benzylidene-3-O-[(R)-(benzyloxycarbonyl)(cyclohexyl)methyl]-β-D-galactopyranosyl}-(1->3)-2-(acetylamino)-4,6-O-benzylidene-2-deoxy-β-D-galactopyranoside

There total 6 articles about thexyldimethylsilyl {4,6-O-benzylidene-3-O-[(R)-(benzyloxycarbonyl)(cyclohexyl)methyl]-β-D-galactopyranosyl}-(1->3)-2-(acetylamino)-4,6-O-benzylidene-2-deoxy-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 866890-20-2
thexyldimethylsilyl {4,6-O-benzylidene-3-O-[(R)-(benzyloxycarbonyl)(cyclohexyl)methyl]-β-D-galactopyranosyl}-(1->3)-2-azido-4,6-O-benzylidene-2-deoxy-β-D-galactopyranoside

: 866890-23-5
thexyldimethylsilyl {4,6-O-benzylidene-3-O-[(R)-(benzyloxycarbonyl)(cyclohexyl)methyl]-β-D-galactopyranosyl}-(1->3)-2-(acetylamino)-4,6-O-benzylidene-2-deoxy-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: propane-1,3-dithiol; pyridine; triethylamine / H₂O / 20 h / 20 °C / pH 9 - 10

2: 138 mg / CH₂Cl₂ / 6 h / 20 °C

With pyridine; 1.3-propanedithiol; triethylamine; In dichloromethane; water;
DOI:10.1080/07328300500176312

Reference yield:

: 100-39-0
benzyl bromide

: 866890-23-5
thexyldimethylsilyl {4,6-O-benzylidene-3-O-[(R)-(benzyloxycarbonyl)(cyclohexyl)methyl]-β-D-galactopyranosyl}-(1->3)-2-(acetylamino)-4,6-O-benzylidene-2-deoxy-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 97 percent / Cs₂CO₃ / dimethylformamide / 16 h / 0 - 20 °C

2: 96 percent / 2,6-lutidine / CH₂Cl₂ / 2.75 h / -78 - 20 °C

3: 164 mg / CsF / 1,2-dimethoxy-ethane; toluene / 3 h / 20 °C

4: propane-1,3-dithiol; pyridine; triethylamine / H₂O / 20 h / 20 °C / pH 9 - 10

5: 138 mg / CH₂Cl₂ / 6 h / 20 °C

With pyridine; 2,6-dimethylpyridine; 1.3-propanedithiol; caesium carbonate; triethylamine; cesium fluoride; In 1,2-dimethoxyethane; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1080/07328300500176312

Reference yield:

: 61475-31-8
(S)-hexahydromandelic acid

: 866890-23-5
thexyldimethylsilyl {4,6-O-benzylidene-3-O-[(R)-(benzyloxycarbonyl)(cyclohexyl)methyl]-β-D-galactopyranosyl}-(1->3)-2-(acetylamino)-4,6-O-benzylidene-2-deoxy-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 97 percent / Cs₂CO₃ / dimethylformamide / 16 h / 0 - 20 °C

2: 96 percent / 2,6-lutidine / CH₂Cl₂ / 2.75 h / -78 - 20 °C

3: 164 mg / CsF / 1,2-dimethoxy-ethane; toluene / 3 h / 20 °C

4: propane-1,3-dithiol; pyridine; triethylamine / H₂O / 20 h / 20 °C / pH 9 - 10

5: 138 mg / CH₂Cl₂ / 6 h / 20 °C

With pyridine; 2,6-dimethylpyridine; 1.3-propanedithiol; caesium carbonate; triethylamine; cesium fluoride; In 1,2-dimethoxyethane; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1080/07328300500176312