(6R,6'R,8R,8'R)-(+)-benzyl-bis(5,6,7,8-tetrahydro-7,7-dimethyl-6,8-methanoquinolin-2-yl)-amine

Base Information

Chemical Name:(6R,6'R,8R,8'R)-(+)-benzyl-bis(5,6,7,8-tetrahydro-7,7-dimethyl-6,8-methanoquinolin-2-yl)-amine
CAS No.:819084-07-6
Molecular Formula:C₃₁H₃₅N₃
Molecular Weight:449.639
Hs Code.:

Synonyms:(6R,6'R,8R,8'R)-(+)-benzyl-bis(5,6,7,8-tetrahydro-7,7-dimethyl-6,8-methanoquinolin-2-yl)-amine

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Chemical Property of (6R,6'R,8R,8'R)-(+)-benzyl-bis(5,6,7,8-tetrahydro-7,7-dimethyl-6,8-methanoquinolin-2-yl)-amine

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Technology Process of (6R,6'R,8R,8'R)-(+)-benzyl-bis(5,6,7,8-tetrahydro-7,7-dimethyl-6,8-methanoquinolin-2-yl)-amine

There total 1 articles about (6R,6'R,8R,8'R)-(+)-benzyl-bis(5,6,7,8-tetrahydro-7,7-dimethyl-6,8-methanoquinolin-2-yl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 100-46-9
benzylamine

: 304857-39-4
(6R,8R)-(-)-2-chloro-5,6,7,8,-tetrahydro-7,7-dimethyl-[6,8-methanoquinoline]

: 819084-07-6
(6R,6'R,8R,8'R)-(+)-benzyl-bis(5,6,7,8-tetrahydro-7,7-dimethyl-6,8-methanoquinolin-2-yl)-amine

Guidance literature:: With 1,3-bis-(diphenylphosphino)propane; bis(dibenzylideneacetone)-palladium⁽⁰⁾; sodium t-butanolate; tetrabutylammomium bromide; In toluene; at 100 ℃;
DOI:10.1016/j.jorganchem.2004.06.032

Reference yield: 93.0%

: copper dichloride

: 819084-07-6
(6R,6'R,8R,8'R)-(+)-benzyl-bis(5,6,7,8-tetrahydro-7,7-dimethyl-6,8-methanoquinolin-2-yl)-amine

: (6R,6'R,8R,8'R)-(+)-benzyl-bis(5,6,7,8-tetrahydro-7,7-dimethyl-6,8-methanoquinolin-2-yl)-amine copper dichloride

Guidance literature:: In ethanol; dichloromethane; (Ar); ligand in CH2Cl2 added to a soln. of anhyd. CuCl2 in abs. EtOH, stirred for 15 min; concd. (vac.), pptd. at 4°C overnight, filtered;
DOI:10.1016/j.jorganchem.2004.06.032