3-benzyloxy-5-tert-butyldiphenylsilyloxybenzyl bromide

Base Information

Chemical Name:3-benzyloxy-5-tert-butyldiphenylsilyloxybenzyl bromide
CAS No.:271580-87-1
Molecular Formula:C₃₀H₃₁BrO₂Si
Molecular Weight:531.564
Hs Code.:

Synonyms:3-benzyloxy-5-tert-butyldiphenylsilyloxybenzyl bromide

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Chemical Property of 3-benzyloxy-5-tert-butyldiphenylsilyloxybenzyl bromide

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Technology Process of 3-benzyloxy-5-tert-butyldiphenylsilyloxybenzyl bromide

There total 4 articles about 3-benzyloxy-5-tert-butyldiphenylsilyloxybenzyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 271580-86-0
3-benzyloxy-5-tert-butyldiphenylsilyloxybenzyl alcohol

: 271580-87-1
3-benzyloxy-5-tert-butyldiphenylsilyloxybenzyl bromide

Guidance literature:: With phosphorus tribromide; In diethyl ether; at 4 ℃;
DOI:10.1016/S0040-4020(00)00078-8

Reference yield:

: 54915-31-0
methyl 3-(benzyloxy)-5-hydroxybenzoate

: 271580-87-1
3-benzyloxy-5-tert-butyldiphenylsilyloxybenzyl bromide

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / imidazole / dimethylformamide / 20 °C

2: 27 percent / LiAlH₄ / diethyl ether / 1 h / Heating

3: 89 percent / PBr₃ / diethyl ether / 4 °C

With 1H-imidazole; lithium aluminium tetrahydride; phosphorus tribromide; In diethyl ether; N,N-dimethyl-formamide; 1: Silylation / 2: Reduction / 3: Substitution;
DOI:10.1016/S0040-4020(00)00078-8

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 271580-87-1
3-benzyloxy-5-tert-butyldiphenylsilyloxybenzyl bromide

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / imidazole / dimethylformamide / 20 °C

2: 27 percent / LiAlH₄ / diethyl ether / 1 h / Heating

3: 89 percent / PBr₃ / diethyl ether / 4 °C

With 1H-imidazole; lithium aluminium tetrahydride; phosphorus tribromide; In diethyl ether; N,N-dimethyl-formamide; 1: Silylation / 2: Reduction / 3: Substitution;
DOI:10.1016/S0040-4020(00)00078-8