2-{4-[4-(benzylamino-diphenyl-methyl)-[1,2,3]triazol-1-yl]-butoxy}-benzoic acid 2-methoxy-ethyl ester

Base Information

Chemical Name:2-{4-[4-(benzylamino-diphenyl-methyl)-[1,2,3]triazol-1-yl]-butoxy}-benzoic acid 2-methoxy-ethyl ester
CAS No.:1263214-82-9
Molecular Formula:C₃₆H₃₈N₄O₄
Molecular Weight:590.722
Hs Code.:

Synonyms:2-{4-[4-(benzylamino-diphenyl-methyl)-[1,2,3]triazol-1-yl]-butoxy}-benzoic acid 2-methoxy-ethyl ester

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Chemical Property of 2-{4-[4-(benzylamino-diphenyl-methyl)-[1,2,3]triazol-1-yl]-butoxy}-benzoic acid 2-methoxy-ethyl ester

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Technology Process of 2-{4-[4-(benzylamino-diphenyl-methyl)-[1,2,3]triazol-1-yl]-butoxy}-benzoic acid 2-methoxy-ethyl ester

There total 8 articles about 2-{4-[4-(benzylamino-diphenyl-methyl)-[1,2,3]triazol-1-yl]-butoxy}-benzoic acid 2-methoxy-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: C₂₉H₃₀ClN₃O₄

: 100-46-9
benzylamine

: 1263214-82-9
2-{4-[4-(benzylamino-diphenyl-methyl)-[1,2,3]triazol-1-yl]-butoxy}-benzoic acid 2-methoxy-ethyl ester

Guidance literature:: With triethylamine; In diethyl ether; dichloromethane; for 2h; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2010.11.026

Reference yield:

: 937021-08-4
benzylcarbamic acid 1,1-dimethylprop-2-ynyl ester

: 1263214-82-9
2-{4-[4-(benzylamino-diphenyl-methyl)-[1,2,3]triazol-1-yl]-butoxy}-benzoic acid 2-methoxy-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; copper(l) iodide / 24 h / 20 °C

2: acetonitrile / pH 4.3 / aq. buffer

3: triethylamine / diethyl ether; dichloromethane / 2 h / Inert atmosphere; Reflux

With pyridine; copper(l) iodide; triethylamine; In diethyl ether; dichloromethane; acetonitrile; 1: Huisgen cycloaddition;
DOI:10.1016/j.tet.2010.11.026

Reference yield:

: 1263214-80-7
2-{4-[4-(benzylcarbamoyloxy-diphenyl-methyl)-[1,2,3]triazol-1-yl]-butoxy}-benzoic acid 2-methoxy-ethyl ester

: 1263214-82-9
2-{4-[4-(benzylamino-diphenyl-methyl)-[1,2,3]triazol-1-yl]-butoxy}-benzoic acid 2-methoxy-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: acetonitrile / pH 4.3 / aq. buffer

2: hydrogenchloride / diethyl ether; dichloromethane / Inert atmosphere

3: triethylamine / diethyl ether; dichloromethane / 2 h / Inert atmosphere; Reflux

With hydrogenchloride; triethylamine; In diethyl ether; dichloromethane; acetonitrile;
DOI:10.1016/j.tet.2010.11.026