Phenylhydrazono-thiomalonsaeure-anilid-nitril

Base Information

• Chemical Name: Phenylhydrazono-thiomalonsaeure-anilid-nitril
• CAS No.: 764657-61-6
• Molecular Formula: C₁₅H₁₂N₄S
• Molecular Weight: 280.353

Synonyms:Phenylhydrazono-thiomalonsaeure-anilid-nitril

Chemical Property of Phenylhydrazono-thiomalonsaeure-anilid-nitril

Chemical Property:

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Technology Process of Phenylhydrazono-thiomalonsaeure-anilid-nitril

There total 2 articles about Phenylhydrazono-thiomalonsaeure-anilid-nitril which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

N-phenylthiocarbamoylacetonitrile (53744-76-6) + benzene diazonium chloride (100-34-5) → Phenylhydrazono-thiomalonsaeure-anilid-nitril (764657-61-6)

Guidance literature:

for 2.5h;

DOI:10.1023/B:COHC.0000010657.14733.8e

Reference yield:

→ Phenylhydrazono-thiomalonsaeure-anilid-nitril (764657-61-6)

Guidance literature:

aus Monothiomalonsaeure-anilid-nitril in A./Natriumacetat u. diazotiertem Anilin;

Reference yield: 94.0%

4-(bromoacetyl)toluene (619-41-0) + Phenylhydrazono-thiomalonsaeure-anilid-nitril (764657-61-6) → [3-amino-4-(phenyl-hydrazono)-5-phenylimino-4,5-dihydro-thiophen-2-yl]-p-tolyl-methanone

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; at 80 ℃; for 34h;

DOI:10.1023/B:COHC.0000010657.14733.8e

upstream raw materials:

N-phenylthiocarbamoylacetonitrile

benzene diazonium chloride

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