N-Trityl-L-glutaminsaeure-γ-methylester * Diethylamin

Base Information

Chemical Name:N-Trityl-L-glutaminsaeure-γ-methylester * Diethylamin
CAS No.:113408-47-2
Molecular Formula:C₄H₁₁N*C₂₅H₂₅NO₄
Molecular Weight:476.616
Hs Code.:

Synonyms:N-Trityl-L-glutaminsaeure-γ-methylester * Diethylamin

Suppliers and Price of N-Trityl-L-glutaminsaeure-γ-methylester * Diethylamin

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
5-Methoxy-5-oxo-N-tritylnorvaline diethylamine
1g
$ 432.00

Matrix Scientific
5-Methoxy-5-oxo-N-tritylnorvaline diethylamine
10g
$ 1602.00

Matrix Scientific
5-Methoxy-5-oxo-N-tritylnorvaline diethylamine
5g
$ 1206.00

American Custom Chemicals Corporation
N-ALPHA-TRITYL-L-GLUTAMIC ACID GAMMA-METHYL ESTER DIETHYLAMMONIUM SALT 95.00%
5MG
$ 496.71

Total 1 raw suppliers

Chemical Property of N-Trityl-L-glutaminsaeure-γ-methylester * Diethylamin

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

5-Methoxy-5-oxo-N-tritylnorvaline diethylamine ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-Trityl-L-glutaminsaeure-γ-methylester * Diethylamin

There total 2 articles about N-Trityl-L-glutaminsaeure-γ-methylester * Diethylamin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1499-55-4
L-glutamic acid 5-methyl ester

: 76-83-5
trityl chloride

: 109-89-7
diethylamine

: 113408-47-2
N-Trityl-L-glutaminsaeure-γ-methylester * Diethylamin

Guidance literature:: L-glutamic acid 5-methyl ester; With chloro-trimethyl-silane; In chloroform; acetonitrile; for 5h; Heating;

trityl chloride; With triethylamine; In chloroform; acetonitrile; at 20 ℃;

diethylamine; With methanol; In chloroform; acetonitrile;
DOI:10.1021/jo035700b

Reference yield:

: 113408-47-2
N-Trityl-L-glutaminsaeure-γ-methylester * Diethylamin

Guidance literature:: N-Trityl-glutaminsaeure-α-trityl-γ-methylester, 1) Eg., 2) Diethylamin;

Reference yield:

: 113408-47-2
N-Trityl-L-glutaminsaeure-γ-methylester * Diethylamin

: (S)-5-Hydroxy-2-{[1-phenyl-meth-(E)-ylidene]-amino}-pentanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: LiAlH₄ / tetrahydrofuran / 2 h / 4 °C

1.2: 1.36 g / AcOH; water / 24 h / 20 °C

2.1: triethylamine / methanol / 2.75 h

With lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; methanol;
DOI:10.1021/jo035700b