1-benzyl-4-[4,4-diphenyl-4-(1-tricyclo[3.3.1.1.(3,7)]decyl)butyl]piperazine

Base Information

Chemical Name:1-benzyl-4-[4,4-diphenyl-4-(1-tricyclo[3.3.1.1.(3,7)]decyl)butyl]piperazine
CAS No.:1427269-26-8
Molecular Formula:C₃₇H₄₆N₂
Molecular Weight:518.786
Hs Code.:

Synonyms:1-benzyl-4-[4,4-diphenyl-4-(1-tricyclo[3.3.1.1.(3,7)]decyl)butyl]piperazine

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Chemical Property of 1-benzyl-4-[4,4-diphenyl-4-(1-tricyclo[3.3.1.1.(3,7)]decyl)butyl]piperazine

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Technology Process of 1-benzyl-4-[4,4-diphenyl-4-(1-tricyclo[3.3.1.1.(3,7)]decyl)butyl]piperazine

There total 4 articles about 1-benzyl-4-[4,4-diphenyl-4-(1-tricyclo[3.3.1.1.(3,7)]decyl)butyl]piperazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 2759-28-6
1-phenylmethylpiperazine

: C₂₇H₃₁F₃O₃S

: 1427269-26-8
1-benzyl-4-[4,4-diphenyl-4-(1-tricyclo[3.3.1.1.(3,7)]decyl)butyl]piperazine

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 1h;
DOI:10.2174/157340612801216201

Reference yield:

: 1427162-90-0
δ,δ-diphenyl-δ-(1-tricyclo[3.3.1.1.(3,7)]decyl)butanol

: 1427269-26-8
1-benzyl-4-[4,4-diphenyl-4-(1-tricyclo[3.3.1.1.(3,7)]decyl)butyl]piperazine

Guidance literature:: Multi-step reaction with 2 steps

1: 2,6-dimethylpyridine / dichloromethane / 1 h / -10 °C / Inert atmosphere

2: tetrahydrofuran / 1 h / 20 °C

With 2,6-dimethylpyridine; In tetrahydrofuran; dichloromethane;
DOI:10.2174/157340612801216201

Reference yield:

: 66951-99-3
α,α-diphenyl-1-tricyclo[3.3.1.1.(3,7)]decanemethanol

: 1427269-26-8
1-benzyl-4-[4,4-diphenyl-4-(1-tricyclo[3.3.1.1.(3,7)]decyl)butyl]piperazine

Guidance literature:: Multi-step reaction with 4 steps

1.1: thionyl chloride; acetyl chloride / 0.5 h / Reflux

2.1: copper(l) iodide / tetrahydrofuran / 4 h / Inert atmosphere; Reflux

2.2: 0 °C / Inert atmosphere

3.1: 2,6-dimethylpyridine / dichloromethane / 1 h / -10 °C / Inert atmosphere

4.1: tetrahydrofuran / 1 h / 20 °C

With 2,6-dimethylpyridine; copper(l) iodide; thionyl chloride; acetyl chloride; In tetrahydrofuran; dichloromethane;
DOI:10.2174/157340612801216201