[RuCl₂(η³:η³-(2,7-dimethylocta-2,6-diene-1,8-diyl)){k¹-(P)-PPh₂(py-6-tert-amyl)}]

Base Information

• Chemical Name: [RuCl₂(η³:η³-(2,7-dimethylocta-2,6-diene-1,8-diyl)){k¹-(P)-PPh₂(py-6-tert-amyl)}]
• CAS No.: 1407534-45-5
• Molecular Formula: C₃₂H₄₀Cl₂NPRu
• Molecular Weight: 641.626

Synonyms:[RuCl₂(η³:η³-(2,7-dimethylocta-2,6-diene-1,8-diyl)){k¹-(P)-PPh₂(py-6-tert-amyl)}]

Chemical Property of [RuCl₂(η³:η³-(2,7-dimethylocta-2,6-diene-1,8-diyl)){k¹-(P)-PPh₂(py-6-tert-amyl)}]

Chemical Property:

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SDS file from LookChem

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Technology Process of [RuCl₂(η³:η³-(2,7-dimethylocta-2,6-diene-1,8-diyl)){k¹-(P)-PPh₂(py-6-tert-amyl)}]

There total 1 articles about [RuCl₂(η³:η³-(2,7-dimethylocta-2,6-diene-1,8-diyl)){k¹-(P)-PPh₂(py-6-tert-amyl)}] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

dichloro-bis-μ-chloro-bis[(1-3η:6-8η)-2,7-dimethyloctadienediyl]diruthenium(II) + 6-tert-amyl-2-diphenylphosphinopyridine (947315-18-6) → [RuCl2(η3:η3-(2,7-dimethylocta-2,6-diene-1,8-diyl)){k1-(P)-PPh2(py-6-tert-amyl)}] (1407534-45-5)

Guidance literature:

In dichloromethane; at 20 ℃; for 0.25h; Inert atmosphere; Schlenk technique;

DOI:10.1002/ejic.201200592

Reference yield: 83.0%

silver hexafluoroantimonate (26042-64-8) + [RuCl2(η3:η3-(2,7-dimethylocta-2,6-diene-1,8-diyl)){k1-(P)-PPh2(py-6-tert-amyl)}] (1407534-45-5) → [RuCl2(η3:η3-(2,7-dimethylocta-2,6-diene-1,8-diyl)){k1-(P)-PPh2(pyH-6-tert-amyl)}][SbF6]

Guidance literature:

In dichloromethane; at 20 ℃; for 24h; Inert atmosphere; Schlenk technique; Darkness;

DOI:10.1016/j.jorganchem.2012.12.027

Reference yield:

chloro(dimethylsulfide) gold(I) (29892-37-3) + [RuCl2(η3:η3-(2,7-dimethylocta-2,6-diene-1,8-diyl)){k1-(P)-PPh2(py-6-tert-amyl)}] (1407534-45-5) → [AuCl{κ1-(P)-PPh2(py-6-tert-amyl)}] (1424152-76-0) + [RuCl2(η3:η3-2,7-dimethylocta-2,6-diene-1,8-diyl)(SMe2)] (1424152-83-9)

Guidance literature:

In dichloromethane; at 20 ℃; for 12h; Inert atmosphere; Schlenk technique;

DOI:10.1016/j.jorganchem.2012.12.027

upstream raw materials:

6-tert-amyl-2-diphenylphosphinopyridine

Downstream raw materials:

[RuCl₂(η³:η³-2,7-dimethylocta-2,6-diene-1,8-diyl)(SMe₂)]

6-tert-amyl-2-diphenylphosphinopyridine

[AuCl{κ¹-(P)-PPh₂(py-6-tert-amyl)}]

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