N-[3-hydroxy-3-(3-methoxyphenyl)propyl]-4-methyl-N-prop-2-ynylbenzenesulfonamide

Base Information

Chemical Name:N-[3-hydroxy-3-(3-methoxyphenyl)propyl]-4-methyl-N-prop-2-ynylbenzenesulfonamide
CAS No.:1378524-22-1
Molecular Formula:C₂₀H₂₃NO₄S
Molecular Weight:373.473
Hs Code.:

Synonyms:N-[3-hydroxy-3-(3-methoxyphenyl)propyl]-4-methyl-N-prop-2-ynylbenzenesulfonamide

Suppliers and Price of N-[3-hydroxy-3-(3-methoxyphenyl)propyl]-4-methyl-N-prop-2-ynylbenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[3-hydroxy-3-(3-methoxyphenyl)propyl]-4-methyl-N-prop-2-ynylbenzenesulfonamide

Chemical Property:

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Technology Process of N-[3-hydroxy-3-(3-methoxyphenyl)propyl]-4-methyl-N-prop-2-ynylbenzenesulfonamide

There total 4 articles about N-[3-hydroxy-3-(3-methoxyphenyl)propyl]-4-methyl-N-prop-2-ynylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1378523-95-5
3-[prop-2-ynyl(toluene-4-sulfonyl)amino]propionic acid prop-2-ynyl ester

: 1378524-22-1
N-[3-hydroxy-3-(3-methoxyphenyl)propyl]-4-methyl-N-prop-2-ynylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: lithium borohydride / tetrahydrofuran; ethanol / 1 h / 5 - 28 °C

2: pyridinium chlorochromate / dichloromethane / 6 h / 10 - 28 °C

3: tetrahydrofuran / 0.92 h / 5 - 28 °C

With lithium borohydride; pyridinium chlorochromate; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1021/ol301219c

Reference yield:

: 187887-01-0
N-(3-hydroxypropyl)-4-methyl-N-prop-2-ynylbenzenesulfonamide

: 1378524-22-1
N-[3-hydroxy-3-(3-methoxyphenyl)propyl]-4-methyl-N-prop-2-ynylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridinium chlorochromate / dichloromethane / 6 h / 10 - 28 °C

2: tetrahydrofuran / 0.92 h / 5 - 28 °C

With pyridinium chlorochromate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol301219c