12-benzyloxy-3,6,9,15-tetraazabicyclo[9.3.1]penta-deca-1⁽¹⁵⁾,11,13-triene hydrochloride

Base Information

• Chemical Name: 12-benzyloxy-3,6,9,15-tetraazabicyclo[9.3.1]penta-deca-1⁽¹⁵⁾,11,13-triene hydrochloride
• CAS No.: 1426819-70-6
• Molecular Formula: C₁₈H₂₄N₄O*ClH
• Molecular Weight: 348.876

Synonyms:12-benzyloxy-3,6,9,15-tetraazabicyclo[9.3.1]penta-deca-1⁽¹⁵⁾,11,13-triene hydrochloride

Chemical Property of 12-benzyloxy-3,6,9,15-tetraazabicyclo[9.3.1]penta-deca-1⁽¹⁵⁾,11,13-triene hydrochloride

Chemical Property:

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Technology Process of 12-benzyloxy-3,6,9,15-tetraazabicyclo[9.3.1]penta-deca-1⁽¹⁵⁾,11,13-triene hydrochloride

There total 6 articles about 12-benzyloxy-3,6,9,15-tetraazabicyclo[9.3.1]penta-deca-1⁽¹⁵⁾,11,13-triene hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

12-benzyloxy-3,6,9-tris(2-nitrobenzenesulfonyl)-3,6,9,15-tetraazabicyclo[9.3.1]penta-deca-(15),11,13-triene (1426819-69-3) → 12-benzyloxy-3,6,9,15-tetraazabicyclo[9.3.1]penta-deca-1(15),11,13-triene hydrochloride (1426819-70-6)

Guidance literature:

12-benzyloxy-3,6,9-tris(2-nitrobenzenesulfonyl)-3,6,9,15-tetraazabicyclo[9.3.1]penta-deca-⁽¹⁵⁾,11,13-triene; With sodium carbonate; thiophenol; In N,N-dimethyl-formamide; at 20 ℃; for 12h;

With hydrogenchloride; In water; N,N-dimethyl-formamide;

DOI:10.1039/c2cc36808k

Reference yield:

4-(benzyloxy)-2,6-bis(hydroxymethyl)pyridine (115148-04-4) → 12-benzyloxy-3,6,9,15-tetraazabicyclo[9.3.1]penta-deca-1(15),11,13-triene hydrochloride (1426819-70-6)

Guidance literature:

Multi-step reaction with 3 steps

1: thionyl chloride / 4 h / 60 °C

2: sodium carbonate / N,N-dimethyl-formamide / 28 h / 100 °C / Inert atmosphere

3: sodium carbonate; thiophenol / N,N-dimethyl-formamide / 12 h / 20 °C

With thionyl chloride; sodium carbonate; thiophenol; In N,N-dimethyl-formamide;

DOI:10.1039/c2cc36808k

Reference yield:

4-(benzyloxy)-2,6-bis(chloromethyl)pyridine (171000-40-1) → 12-benzyloxy-3,6,9,15-tetraazabicyclo[9.3.1]penta-deca-1(15),11,13-triene hydrochloride (1426819-70-6)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium carbonate / N,N-dimethyl-formamide / 28 h / 100 °C / Inert atmosphere

2: sodium carbonate; thiophenol / N,N-dimethyl-formamide / 12 h / 20 °C

With sodium carbonate; thiophenol; In N,N-dimethyl-formamide;

DOI:10.1039/c2cc36808k

upstream raw materials:

4-(benzyloxy)-2,6-bis(hydroxymethyl)pyridine

4-(benzyloxy)-2,6-bis(chloromethyl)pyridine

12-benzyloxy-3,6,9-tris(2-nitrobenzenesulfonyl)-3,6,9,15-tetraazabicyclo[9.3.1]penta-deca-⁽¹⁵⁾,11,13-triene

4-hydroxypyridine-2,6-dicarboxylic acid diethylester

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