Diethyl- 4-hydroxy- 2,6-pyridinedicarboxylate, 或4-Hydroxy-2,6-pyridinedicarboxylic acid diethyl ester

Base Information

• Chemical Name: Diethyl- 4-hydroxy- 2,6-pyridinedicarboxylate, 或4-Hydroxy-2,6-pyridinedicarboxylic acid diethyl ester
• CAS No.: 68631-52-7
• Molecular Formula: C11H13NO5
• Molecular Weight: 239.228
• Hs Code.: 2933399090
• Mol file: 68631-52-7.mol

Synonyms:diethyl 4-hydroxypyridine-2,6-dicarboxylic acid;4-hydroxy-pyridine-3-sulfonic acid;4-HYDROXYPYRIDIE-SULPHONIC ACID;4-hydroxypyridine-3-sulfonyl acid;4-hydroxypyridine-2,6-dicarboxylic acid diethyl ester;4-Hydroxypyridine-3-sulphonic;4-HYDROXYPYRIDIE-3-SULPHONIC ACID;hydroxypyridinesulfonicacid;2,6-diethyl-4-hydroxypyridine-2,6-dicarboxylate;4-Hydroxy-3-pyridinesulfonic;4-hydroxypyridin-3-sulfonic acid;4-hydroxypyridine-3-sulphonic acid;diethyl 4-hydroxypyridine-2,6-dicarboxylate;4-HYDROXY-3-PYRIDINESULFONIC ACID;4-Hydroxy-pyridin-3-sulfonsaeure;4-Hydroxypyridine-sulphonic acid;4-PYRIDINOL-3-SULFONIC ACID;

Chemical Property of Diethyl- 4-hydroxy- 2,6-pyridinedicarboxylate, 或4-Hydroxy-2,6-pyridinedicarboxylic acid diethyl ester

Chemical Property:

• PSA: 85.46000
• LogP: 0.72830
• Storage Temp.: Inert atmosphere,Room Temperature

Purity/Quality:

99%, ^*data from raw suppliers

Diethyl4-hydroxypyridine-2,6-dicarboxylate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Diethyl- 4-hydroxy- 2,6-pyridinedicarboxylate, 或4-Hydroxy-2,6-pyridinedicarboxylic acid diethyl ester

There total 9 articles about Diethyl- 4-hydroxy- 2,6-pyridinedicarboxylate, 或4-Hydroxy-2,6-pyridinedicarboxylic acid diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

Chelidamic acid (499-51-4) + ethanol (64-17-5) → 4-hydroxypyridine-2,6-dicarboxylic acid diethylester (68631-52-7)

Guidance literature:

With thionyl chloride; for 2h; Heating;

DOI:10.1021/ja039230e

Reference yield: 99.0%

chelidamic acid + ethanol (64-17-5) → 4-hydroxypyridine-2,6-dicarboxylic acid diethylester (68631-52-7)

Guidance literature:

chelidamic acid; ethanol; With thionyl chloride; at 20 ℃; for 20h;

for 2h; Further stages.; Heating;

DOI:10.1021/ja0289548

Reference yield: 98.0%

ethanol (64-17-5) + chelidamic acid (138-60-3) → 4-hydroxypyridine-2,6-dicarboxylic acid diethylester (68631-52-7)

Guidance literature:

With thionyl chloride; at 20 - 80 ℃; for 20h; Inert atmosphere; Reflux;

DOI:10.1055/s-0034-1379549

upstream raw materials:

Chelidamic acid

ethanol

ethyl iodide

chelidamic acid

Downstream raw materials:

C₃₆H₃₇N₃O₁₁

C₆H₅CH₂OC₅NH₂[CH₂SC₆H₄CH₂OC₅NH₂(COOC₂H₅)2]2

4-ethoxy-2,6-pyridinedicarboxylate d'ethyle

C₄₇H₅₈N₆O₁₈

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