C₃₃H₄₆N₂O₆SSi

Base Information

Chemical Name:C₃₃H₄₆N₂O₆SSi
CAS No.:130253-37-1
Molecular Formula:C₃₃H₄₆N₂O₆SSi
Molecular Weight:626.89
Hs Code.:

C<sub>33</sub>H<sub>46</sub>N<sub>2</sub>O<sub>6</sub>SSi

Synonyms:C₃₃H₄₆N₂O₆SSi

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Chemical Property of C₃₃H₄₆N₂O₆SSi

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Technology Process of C₃₃H₄₆N₂O₆SSi

There total 12 articles about C₃₃H₄₆N₂O₆SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 130253-43-9
C₃₂H₄₄N₂O₄Si

: 124-63-0
methanesulfonyl chloride

: 130253-37-1
C₃₃H₄₆N₂O₆SSi

Guidance literature:: With dmap; triethylamine; In dichloromethane;
DOI:10.1016/S0040-4039(00)88787-0

Reference yield:

: C₂₈H₃₀N₂O₅

: 130253-37-1
C₃₃H₄₆N₂O₆SSi

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / NaBH₄ / methanol / 0 °C

2: 80 percent / Et₃N / CH₂Cl₂

3: 90 percent / aq. KOH / methanol

4: 93 percent / Et₃N, DMAP / CH₂Cl₂

With dmap; potassium hydroxide; sodium tetrahydroborate; triethylamine; In methanol; dichloromethane;
DOI:10.1016/S0040-4039(00)88787-0

Reference yield:

: 130278-17-0
C₂₉H₃₄N₂O₅

: 130253-37-1
C₃₃H₄₆N₂O₆SSi

Guidance literature:: Multi-step reaction with 7 steps

1: 90 percent / CH₂Cl₂

2: 68 percent / Pb(OAc)4 / CH₂Cl₂ / -70 °C

3: AcOH / tetrahydrofuran; H₂O / Ambient temperature

4: 80 percent / NaBH₄ / methanol / 0 °C

5: 80 percent / Et₃N / CH₂Cl₂

6: 90 percent / aq. KOH / methanol

7: 93 percent / Et₃N, DMAP / CH₂Cl₂

With lead(IV) acetate; dmap; potassium hydroxide; sodium tetrahydroborate; acetic acid; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1016/S0040-4039(00)88787-0