C₂₇H₂₅ClN₂O₅

Base Information

Chemical Name:C₂₇H₂₅ClN₂O₅
CAS No.:1423690-66-7
Molecular Formula:C₂₇H₂₅ClN₂O₅
Molecular Weight:492.959
Hs Code.:

C<sub>27</sub>H<sub>25</sub>ClN<sub>2</sub>O<sub>5</sub>

Synonyms:C₂₇H₂₅ClN₂O₅

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Chemical Property of C₂₇H₂₅ClN₂O₅

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Technology Process of C₂₇H₂₅ClN₂O₅

There total 9 articles about C₂₇H₂₅ClN₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.2%

: 1423702-34-4
C₁₈H₁₈N₂O₃

: 13524-04-4,131864-71-6,132437-66-2,120466-66-2
(R)-1-(o-chlorophenyl)ethanol

: 7693-46-1
4-Nitrophenyl chloroformate

: 1423690-66-7
C₂₇H₂₅ClN₂O₅

Guidance literature:: C₁₈H₁₈N₂O₃; 4-Nitrophenyl chloroformate; With pyridine; In 1,2-dichloro-ethane; at 0 - 20 ℃; for 1h; Inert atmosphere;

(R)-1-(o-chlorophenyl)ethanol; In 1,2-dichloro-ethane; at 80 ℃; Inert atmosphere;

Reference yield:

: 2142-68-9
1-(2-chlorophenyl)ethanone

: 1423690-66-7
C₂₇H₂₅ClN₂O₅

Guidance literature:: Multi-step reaction with 2 steps

1.1: (S)-tetrahydro-1-butyl-3,3-diphenyl-1H,3H-pyrrolo{2,1-c}{1,3,2}oxazaborole; dimethylsulfide borane complex / tetrahydrofuran / 0.5 h / 20 °C

2.1: pyridine / 1,2-dichloro-ethane / 1 h / 0 - 20 °C / Inert atmosphere

2.2: 80 °C / Inert atmosphere

With pyridine; dimethylsulfide borane complex; (S)-tetrahydro-1-butyl-3,3-diphenyl-1H,3H-pyrrolo{2,1-c}{1,3,2}oxazaborole; In tetrahydrofuran; 1,2-dichloro-ethane;

Reference yield:

: 909389-74-8
acetic acid 3,5-dibromo-phenyl ester

: 1423690-66-7
C₂₇H₂₅ClN₂O₅

Guidance literature:: Multi-step reaction with 9 steps

1.1: aluminum (III) chloride / 3 h / 160 °C / Inert atmosphere

2.1: sodium carbonate / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

3.1: pyridine; hydroxylamine hydrochloride / 6 h / 130 °C / Inert atmosphere

4.1: N,N`-dimethylethylenediamine; sodium t-butanolate; copper(l) iodide / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

5.1: boron tribromide / dichloromethane / 0 °C / Inert atmosphere

6.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,2-dimethoxyethane / 80 °C / Inert atmosphere

7.1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

8.1: palladium diacetate; caesium carbonate; Benzophenone imine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / tetrahydrofuran / 80 °C / Inert atmosphere

9.1: pyridine / 1,2-dichloro-ethane / 1 h / 0 - 20 °C / Inert atmosphere

9.2: 80 °C / Inert atmosphere

With pyridine; Benzophenone imine; aluminum (III) chloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide; hydroxylamine hydrochloride; palladium diacetate; boron tribromide; sodium carbonate; caesium carbonate; triethylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate; N,N`-dimethylethylenediamine; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;