ethyl 2-{methyl-[2-(methyl-phenyl-thiocarbamoyl)-acetyl]-amino}-5-pyrrol-1-yl-benzoate

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Chemical Name:ethyl 2-{methyl-[2-(methyl-phenyl-thiocarbamoyl)-acetyl]-amino}-5-pyrrol-1-yl-benzoate
CAS No.:172896-66-1
Molecular Formula:C₂₄H₂₅N₃O₃S
Molecular Weight:435.547
Hs Code.:

Synonyms:ethyl 2-{methyl-[2-(methyl-phenyl-thiocarbamoyl)-acetyl]-amino}-5-pyrrol-1-yl-benzoate

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Chemical Property of ethyl 2-{methyl-[2-(methyl-phenyl-thiocarbamoyl)-acetyl]-amino}-5-pyrrol-1-yl-benzoate

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Technology Process of ethyl 2-{methyl-[2-(methyl-phenyl-thiocarbamoyl)-acetyl]-amino}-5-pyrrol-1-yl-benzoate

There total 2 articles about ethyl 2-{methyl-[2-(methyl-phenyl-thiocarbamoyl)-acetyl]-amino}-5-pyrrol-1-yl-benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 172896-85-4
N-methyl-N-phenylthiocarbamoylacetic acid

: 2-methylamino-5-pyrrol-1-yl-benzoic acid ethyl ester

: 172896-66-1
ethyl 2-{methyl-[2-(methyl-phenyl-thiocarbamoyl)-acetyl]-amino}-5-pyrrol-1-yl-benzoate

Guidance literature:: With pyridine; 4 A molecular sieve; pivaloyl chloride; In dichloromethane; at -20 - 20 ℃;
DOI:10.1002/jhet.5570390427

Reference yield:

: 64-17-5
ethanol

: 172896-85-4
N-methyl-N-phenylthiocarbamoylacetic acid

: 1-methyl-6-pyrrol-1-yl-1H-benzo[d][1,3]oxazine-2,4-dione

: 172896-66-1
ethyl 2-{methyl-[2-(methyl-phenyl-thiocarbamoyl)-acetyl]-amino}-5-pyrrol-1-yl-benzoate

Guidance literature:: ethanol; 1-methyl-6-pyrrol-1-yl-1H-benzo[d][1,3]oxazine-2,4-dione; With sodium ethanolate; Heating;

N-methyl-N-phenylthiocarbamoylacetic acid; With pyridine; pivaloyl chloride; In dichloromethane; at 20 ℃;
DOI:10.1016/S0960-894X(02)00377-3