Diphenyl-N-(benzyloxyacrbonyl)-L-alanyl-(2-decarboxyglycin-2-yl)phosphonat

Base Information

Chemical Name:Diphenyl-N-(benzyloxyacrbonyl)-L-alanyl-(2-decarboxyglycin-2-yl)phosphonat
CAS No.:104173-21-9
Molecular Formula:C₂₄H₂₅N₂O₆P
Molecular Weight:468.446
Hs Code.:

Synonyms:Diphenyl-N-(benzyloxyacrbonyl)-L-alanyl-(2-decarboxyglycin-2-yl)phosphonat

Suppliers and Price of Diphenyl-N-(benzyloxyacrbonyl)-L-alanyl-(2-decarboxyglycin-2-yl)phosphonat

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Diphenyl-N-(benzyloxyacrbonyl)-L-alanyl-(2-decarboxyglycin-2-yl)phosphonat

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Technology Process of Diphenyl-N-(benzyloxyacrbonyl)-L-alanyl-(2-decarboxyglycin-2-yl)phosphonat

There total 2 articles about Diphenyl-N-(benzyloxyacrbonyl)-L-alanyl-(2-decarboxyglycin-2-yl)phosphonat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 101-02-0
triphenyl phosphite

: 104173-18-4
N²-(Benzyloxycarbonyl)-N¹-(methoxymethyl)-L-alaninamid

: 104173-21-9
Diphenyl-N-(benzyloxyacrbonyl)-L-alanyl-(2-decarboxyglycin-2-yl)phosphonat

Guidance literature:: With titanium tetrachloride;

Reference yield:

: 2503-31-3,3235-17-4,34286-66-3
N-benzyloxycarbonyl-L-alanylglycine

: 104173-21-9
Diphenyl-N-(benzyloxyacrbonyl)-L-alanyl-(2-decarboxyglycin-2-yl)phosphonat

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / Et₃N / anodic oxidation; Pt electrodes, i = 200 mA*cm^-2, current equiv.: 2.2 F/mol

2: 59 percent / TiCL₄ / CH₂Cl₂ / 10 h / -78 deg C -> room temperature

With titanium tetrachloride; triethylamine; In dichloromethane;
DOI:10.1002/hlca.19890720302