4-methybenzophenone dimethyl acetal

Base Information

• Chemical Name: 4-methybenzophenone dimethyl acetal
• CAS No.: 1190071-11-4
• Molecular Formula: C₁₆H₁₈O₂
• Molecular Weight: 242.318

Synonyms:4-methybenzophenone dimethyl acetal

Chemical Property of 4-methybenzophenone dimethyl acetal

Chemical Property:

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Technology Process of 4-methybenzophenone dimethyl acetal

There total 1 articles about 4-methybenzophenone dimethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

4-Methylbenzophenone (134-84-9) + trimethyl orthoformate (149-73-5) → 4-methybenzophenone dimethyl acetal (1190071-11-4)

Guidance literature:

With ytterbium(III) triflate; In methanol; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1002/ejoc.200900566

Reference yield: 99.0%

dibutyl disulfide (629-45-8) + 4-methybenzophenone dimethyl acetal (1190071-11-4) → 1-methyl-4-[phenyl(butylthio)methyl]-benzene (84811-73-4)

Guidance literature:

With triethylsilane; indium(III) bromide; In toluene; at 100 ℃; for 1h; Inert atmosphere;

DOI:10.1002/ejoc.200900566

upstream raw materials:

4-Methylbenzophenone

trimethyl orthoformate

Downstream raw materials:

1-methyl-4-[phenyl(butylthio)methyl]-benzene

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