(E)-ethyl-2-((4-(trifluoromethyl)phenyl)(triethylsiloxy)methyl)-3-iodoacrylate

Base Information

Chemical Name:(E)-ethyl-2-((4-(trifluoromethyl)phenyl)(triethylsiloxy)methyl)-3-iodoacrylate
CAS No.:1170303-26-0
Molecular Formula:C₁₉H₂₆F₃IO₃Si
Molecular Weight:514.399
Hs Code.:

Synonyms:(E)-ethyl-2-((4-(trifluoromethyl)phenyl)(triethylsiloxy)methyl)-3-iodoacrylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-ethyl-2-((4-(trifluoromethyl)phenyl)(triethylsiloxy)methyl)-3-iodoacrylate

Chemical Property:

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Technology Process of (E)-ethyl-2-((4-(trifluoromethyl)phenyl)(triethylsiloxy)methyl)-3-iodoacrylate

There total 1 articles about (E)-ethyl-2-((4-(trifluoromethyl)phenyl)(triethylsiloxy)methyl)-3-iodoacrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: ethyl (E)-2-((4-trifluoromethylphenyl)(hydroxy)methyl)-3-iodoacrylate

: 994-30-9
triethylsilyl chloride

: 1170303-26-0
(E)-ethyl-2-((4-(trifluoromethyl)phenyl)(triethylsiloxy)methyl)-3-iodoacrylate

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 8h;

Reference yield: 83.0%

: 1170303-26-0
(E)-ethyl-2-((4-(trifluoromethyl)phenyl)(triethylsiloxy)methyl)-3-iodoacrylate

: 117711-00-9
tridecylmagnesium bromide

: 1170303-27-1
(E)-ethyl-2-((4-trifluoromethylphenyl)(triethylsiloxy)methyl)hexadeca-2-enoate

Guidance literature:: lithium copper bromide; In tetrahydrofuran; at -30 ℃;

Reference yield:

: 1170303-26-0
(E)-ethyl-2-((4-(trifluoromethyl)phenyl)(triethylsiloxy)methyl)-3-iodoacrylate

: 1170303-18-0
(E)-ethyl-2-((4-(trifluoromethyl)phenyl)(hydroxy)methyl)hexadeca-2-enoate

Guidance literature:: Multi-step reaction with 2 steps

1: lithium copper bromide / tetrahydrofuran / -30 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / -30 °C

With tetrabutyl ammonium fluoride; lithium copper bromide; In tetrahydrofuran;