C₆₆H₄₅N₃

Base Information

Chemical Name:C₆₆H₄₅N₃
CAS No.:1285719-61-0
Molecular Formula:C₆₆H₄₅N₃
Molecular Weight:880.103
Hs Code.:

C<sub>66</sub>H<sub>45</sub>N<sub>3</sub>

Synonyms:C₆₆H₄₅N₃

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Chemical Property of C₆₆H₄₅N₃

Chemical Property:

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Technology Process of C₆₆H₄₅N₃

There total 5 articles about C₆₆H₄₅N₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1762-84-1
4-bromo-p-terphenyl

: 1285719-50-7
C₄₈H₃₃N₃

: 1285719-61-0
C₆₆H₄₅N₃

Guidance literature:: With sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butyl phosphine; In toluene; at 80 ℃; for 8h; Inert atmosphere;

Reference yield:

: 1150-62-5
N-phenylcarbazole

: 1285719-61-0
C₆₆H₄₅N₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium iodide; sulfuric acid; potassium iodate / ethanol / 2 h / 75 °C

2.1: n-butyllithium / toluene; hexane; diethyl ether / 1 h / -45 - -5 °C / Inert atmosphere

2.2: 2 h / -45 °C / Inert atmosphere

2.3: 20 °C / Inert atmosphere

3.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; water / 10 h / Inert atmosphere; Reflux

4.1: potassium carbonate; copper(l) iodide; acetamide / ortho-diethylbenzene / 38 h / 175 °C / Inert atmosphere

4.2: 5 h / 175 °C

5.1: sodium t-butanolate / tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 8 h / 80 °C / Inert atmosphere

With acetamide; potassium iodate; copper(l) iodide; n-butyllithium; sulfuric acid; sodium carbonate; potassium carbonate; potassium iodide; sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; In diethyl ether; ethanol; hexane; ortho-diethylbenzene; water; toluene;

Reference yield:

: 502161-03-7
3-iodo-9-phenyl-9H-carbazole

: 1285719-61-0
C₆₆H₄₅N₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / toluene; hexane; diethyl ether / 1 h / -45 - -5 °C / Inert atmosphere

1.2: 2 h / -45 °C / Inert atmosphere

1.3: 20 °C / Inert atmosphere

2.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; water / 10 h / Inert atmosphere; Reflux

3.1: potassium carbonate; copper(l) iodide; acetamide / ortho-diethylbenzene / 38 h / 175 °C / Inert atmosphere

3.2: 5 h / 175 °C

4.1: sodium t-butanolate / tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 8 h / 80 °C / Inert atmosphere

With acetamide; copper(l) iodide; n-butyllithium; sodium carbonate; potassium carbonate; sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; In diethyl ether; hexane; ortho-diethylbenzene; water; toluene;