O-(2-azido-6-O-benzoyl-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->6)-2,3:4,5-di-O-cyclohexylidene-1-O-(1R)-menthyloxycarbonyl-D-myoinositol

Base Information

Chemical Name:O-(2-azido-6-O-benzoyl-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->6)-2,3:4,5-di-O-cyclohexylidene-1-O-(1R)-menthyloxycarbonyl-D-myoinositol
CAS No.:164070-36-4
Molecular Formula:C₄₉H₆₅N₃O₁₃
Molecular Weight:904.067
Hs Code.:

Synonyms:O-(2-azido-6-O-benzoyl-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->6)-2,3:4,5-di-O-cyclohexylidene-1-O-(1R)-menthyloxycarbonyl-D-myoinositol

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Chemical Property of O-(2-azido-6-O-benzoyl-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->6)-2,3:4,5-di-O-cyclohexylidene-1-O-(1R)-menthyloxycarbonyl-D-myoinositol

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Technology Process of O-(2-azido-6-O-benzoyl-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->6)-2,3:4,5-di-O-cyclohexylidene-1-O-(1R)-menthyloxycarbonyl-D-myoinositol

There total 5 articles about O-(2-azido-6-O-benzoyl-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->6)-2,3:4,5-di-O-cyclohexylidene-1-O-(1R)-menthyloxycarbonyl-D-myoinositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 100-39-0
benzyl bromide

: O-(2-azido-6-O-benzoyl-2-deoxy-α-D-glucopyranosyl)-(1->6)-2,3:4,5-di-O-cyclohexylidene-1-O-(1R)-menthyloxycarbonyl-D-myoinositol

: 164070-36-4
O-(2-azido-6-O-benzoyl-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->6)-2,3:4,5-di-O-cyclohexylidene-1-O-(1R)-menthyloxycarbonyl-D-myoinositol

Guidance literature:: With 3 A molecular sieve; silver(l) oxide;

Reference yield:

: 202812-14-4
O-(2-azido-2-deoxy-α-D-glucopyranosyl)-(1->6)-2,3:4,5-di-O-cyclohexylidene-1-O-(1R)-menthyloxycarbonyl-D-myoinositol

: 164070-36-4
O-(2-azido-6-O-benzoyl-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->6)-2,3:4,5-di-O-cyclohexylidene-1-O-(1R)-menthyloxycarbonyl-D-myoinositol

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / Et₃N / acetonitrile; diethyl ether / 2 h / -60 °C

2: 73 percent / Ag₂O, molecular sieves (3 Angstroem) / CH₂Cl₂ / 18 h / Ambient temperature

With 3 A molecular sieve; triethylamine; silver(l) oxide; In diethyl ether; dichloromethane; acetonitrile;
DOI:10.1002/(SICI)1099-0690(199905)1999:5<1153::AID-EJOC1153>3.0.CO;2-S

Reference yield:

: 613-90-1
benzoyl cyanide

: 164070-36-4
O-(2-azido-6-O-benzoyl-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->6)-2,3:4,5-di-O-cyclohexylidene-1-O-(1R)-menthyloxycarbonyl-D-myoinositol

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / Et₃N / acetonitrile; diethyl ether / 2 h / -60 °C

2: 73 percent / Ag₂O, molecular sieves (3 Angstroem) / CH₂Cl₂ / 18 h / Ambient temperature

With 3 A molecular sieve; triethylamine; silver(l) oxide; In diethyl ether; dichloromethane; acetonitrile;
DOI:10.1002/(SICI)1099-0690(199905)1999:5<1153::AID-EJOC1153>3.0.CO;2-S