<4-<4-<<4-<(2-methyl-1-oxopropyl)amino>phneyl>oxoacetyl>-1-piperazinyl>-4-oxobutyl>carbamic acid phenylmethyl ester

Base Information

Chemical Name:<4-<4-<<4-<(2-methyl-1-oxopropyl)amino>phneyl>oxoacetyl>-1-piperazinyl>-4-oxobutyl>carbamic acid phenylmethyl ester
CAS No.:219661-61-7
Molecular Formula:C₂₈H₃₄N₄O₆
Molecular Weight:522.601
Hs Code.:

Synonyms:<4-<4-<<4-<(2-methyl-1-oxopropyl)amino>phneyl>oxoacetyl>-1-piperazinyl>-4-oxobutyl>carbamic acid phenylmethyl ester

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Chemical Property of <4-<4-<<4-<(2-methyl-1-oxopropyl)amino>phneyl>oxoacetyl>-1-piperazinyl>-4-oxobutyl>carbamic acid phenylmethyl ester

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Technology Process of <4-<4-<<4-<(2-methyl-1-oxopropyl)amino>phneyl>oxoacetyl>-1-piperazinyl>-4-oxobutyl>carbamic acid phenylmethyl ester

There total 4 articles about <4-<4-<<4-<(2-methyl-1-oxopropyl)amino>phneyl>oxoacetyl>-1-piperazinyl>-4-oxobutyl>carbamic acid phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 219661-56-0
4-<(2-methyl-1-oxopropyl)amino>-α-oxo-benzeneacetic acid

: 219661-60-6
<4-oxo-4-(piperazinyl)butyl>carbamic acid phenylmethyl ester

: 219661-61-7
<4-<4-<<4-<(2-methyl-1-oxopropyl)amino>phneyl>oxoacetyl>-1-piperazinyl>-4-oxobutyl>carbamic acid phenylmethyl ester

Guidance literature:: With bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine; In chloroform; for 3h; Ambient temperature;
DOI:10.1021/ja982711r

Reference yield:

: 5105-78-2
4-(benzyloxycarbonylamino)butyric acid

: 219661-61-7
<4-<4-<<4-<(2-methyl-1-oxopropyl)amino>phneyl>oxoacetyl>-1-piperazinyl>-4-oxobutyl>carbamic acid phenylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) HOBt, EDC / 1.) DMF, 30 min, 2.) DMF

2: 51 percent / Et₃N, bis(2-oxo-3-oxazolidinyl)phosphinic chloride / CHCl₃ / 3 h / Ambient temperature

With bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; In chloroform;
DOI:10.1021/ja982711r

Reference yield:

: 99-92-3
p-aminobenzophenone

: 219661-61-7
<4-<4-<<4-<(2-methyl-1-oxopropyl)amino>phneyl>oxoacetyl>-1-piperazinyl>-4-oxobutyl>carbamic acid phenylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / Et₃N / CH₂Cl₂ / 1 h / Ambient temperature

2: 85 percent / SeO₂, pyridine / 14 h / 100 °C

3: 51 percent / Et₃N, bis(2-oxo-3-oxazolidinyl)phosphinic chloride / CHCl₃ / 3 h / Ambient temperature

With pyridine; selenium(IV) oxide; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine; In dichloromethane; chloroform;
DOI:10.1021/ja982711r