10-(benzyloxy)-2,2-dimethyl-1,3,6-trioxaspiro(4,5)decane-8,9-diol

Base Information

Chemical Name:10-(benzyloxy)-2,2-dimethyl-1,3,6-trioxaspiro(4,5)decane-8,9-diol
CAS No.:70551-32-5
Molecular Formula:C₁₆H₂₂O₆
Molecular Weight:310.347
Hs Code.:

Synonyms:10-(benzyloxy)-2,2-dimethyl-1,3,6-trioxaspiro(4,5)decane-8,9-diol

Suppliers and Price of 10-(benzyloxy)-2,2-dimethyl-1,3,6-trioxaspiro(4,5)decane-8,9-diol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 10-(benzyloxy)-2,2-dimethyl-1,3,6-trioxaspiro(4,5)decane-8,9-diol

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 10-(benzyloxy)-2,2-dimethyl-1,3,6-trioxaspiro(4,5)decane-8,9-diol

There total 8 articles about 10-(benzyloxy)-2,2-dimethyl-1,3,6-trioxaspiro(4,5)decane-8,9-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 85458-76-0
3-O-Benzyl-1,2:4,5-di-O-isopropylidene-β-D-fructopyranose

: 70551-32-5
10-(benzyloxy)-2,2-dimethyl-1,3,6-trioxaspiro(4,5)decane-8,9-diol

Guidance literature:: With acetic acid; for 12h; Ambient temperature;
DOI:10.1021/jo00108a018

Reference yield: 85.0%

: 1125824-35-2
C₂₃H₂₆O₆

: 70551-32-5
10-(benzyloxy)-2,2-dimethyl-1,3,6-trioxaspiro(4,5)decane-8,9-diol

Guidance literature:: With phosphomolybdic acid; silica gel; In dichloromethane; at 20 ℃; for 3h; chemoselective reaction;
DOI:10.1002/ejoc.200800963

Reference yield:

: 25018-67-1
1,2;4,5-di-O-isopropylidene-β-D-(-)-fructopyranose

: 70551-32-5
10-(benzyloxy)-2,2-dimethyl-1,3,6-trioxaspiro(4,5)decane-8,9-diol

Guidance literature:: Multi-step reaction with 2 steps

1: NaH / dimethylformamide

2: aq. AcOH

With sodium hydride; acetic acid; In N,N-dimethyl-formamide;
DOI:10.1055/s-2005-923583