benzyl 2-[[(3R)-3-benzyl-3-(tertbutoxycarbonylamino)-2-oxoazetidin1-yl]dimethylacetamido]-2-methylpropanoate

Base Information

Chemical Name:benzyl 2-[[(3R)-3-benzyl-3-(tertbutoxycarbonylamino)-2-oxoazetidin1-yl]dimethylacetamido]-2-methylpropanoate
CAS No.:1415380-25-4
Molecular Formula:C₃₀H₃₉N₃O₆
Molecular Weight:537.656
Hs Code.:

Synonyms:benzyl 2-[[(3R)-3-benzyl-3-(tertbutoxycarbonylamino)-2-oxoazetidin1-yl]dimethylacetamido]-2-methylpropanoate

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Chemical Property of benzyl 2-[[(3R)-3-benzyl-3-(tertbutoxycarbonylamino)-2-oxoazetidin1-yl]dimethylacetamido]-2-methylpropanoate

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Technology Process of benzyl 2-[[(3R)-3-benzyl-3-(tertbutoxycarbonylamino)-2-oxoazetidin1-yl]dimethylacetamido]-2-methylpropanoate

There total 3 articles about benzyl 2-[[(3R)-3-benzyl-3-(tertbutoxycarbonylamino)-2-oxoazetidin1-yl]dimethylacetamido]-2-methylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1415380-25-4
benzyl 2-[[(3R)-3-benzyl-3-(tertbutoxycarbonylamino)-2-oxoazetidin1-yl]dimethylacetamido]-2-methylpropanoate

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 16 h / 20 °C / Inert atmosphere

2: lithium hydroxide monohydrate; water / methanol / 4 h / 20 °C / Inert atmosphere

3: N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline / 16 h / -12 - 20 °C / Inert atmosphere

With lithium hydroxide monohydrate; water; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; In methanol; dichloromethane;
DOI:10.1021/jo302368y

Reference yield:

: 1415380-23-2
(3R)-3-benzyl-3-tert-butoxycarbonyl-1-[1-(methoxycarbonyl)isopropyl]azetidin-2-one

: 1415380-25-4
benzyl 2-[[(3R)-3-benzyl-3-(tertbutoxycarbonylamino)-2-oxoazetidin1-yl]dimethylacetamido]-2-methylpropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: lithium hydroxide monohydrate; water / methanol / 4 h / 20 °C / Inert atmosphere

2: N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline / 16 h / -12 - 20 °C / Inert atmosphere

With lithium hydroxide monohydrate; water; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; In methanol;
DOI:10.1021/jo302368y