5-[4-(benzyloxycarbonylamino)butyrylamino]-m-xylylenebis(phosphonic acid) tetramethyl ester

Base Information

Chemical Name:5-[4-(benzyloxycarbonylamino)butyrylamino]-m-xylylenebis(phosphonic acid) tetramethyl ester
CAS No.:866547-20-8
Molecular Formula:C₂₄H₃₄N₂O₉P₂
Molecular Weight:556.489
Hs Code.:

Synonyms:5-[4-(benzyloxycarbonylamino)butyrylamino]-m-xylylenebis(phosphonic acid) tetramethyl ester

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Chemical Property of 5-[4-(benzyloxycarbonylamino)butyrylamino]-m-xylylenebis(phosphonic acid) tetramethyl ester

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Technology Process of 5-[4-(benzyloxycarbonylamino)butyrylamino]-m-xylylenebis(phosphonic acid) tetramethyl ester

There total 1 articles about 5-[4-(benzyloxycarbonylamino)butyrylamino]-m-xylylenebis(phosphonic acid) tetramethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 5105-78-2
4-(benzyloxycarbonylamino)butyric acid

: 262863-45-6
5-amino-m-xylylenebis(phosphonic acid) tetramethyl ester

: 866547-20-8
5-[4-(benzyloxycarbonylamino)butyrylamino]-m-xylylenebis(phosphonic acid) tetramethyl ester

Guidance literature:: With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine; In dichloromethane; ethyl acetate; at 20 ℃; for 16h;
DOI:10.1002/anie.200462702

Reference yield: 99.0%

: 866547-20-8
5-[4-(benzyloxycarbonylamino)butyrylamino]-m-xylylenebis(phosphonic acid) tetramethyl ester

: 5-[4-(benzyloxycarbonylamino)butyrylamino]-m-xylylenebis(phosphonic acid) dimethyl ester dilithium salt

Guidance literature:: With lithium bromide; In acetonitrile; at 80 ℃; for 48h;
DOI:10.1002/anie.200462702

Reference yield:

: 866547-20-8
5-[4-(benzyloxycarbonylamino)butyrylamino]-m-xylylenebis(phosphonic acid) tetramethyl ester

: 5-[4-aminobutyrylamino]-m-xylylenebis(phosphonic acid) dimethyl ester dilithium salt

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / LiBr / acetonitrile / 48 h / 80 °C

2: 99 percent / H₂ / Pd/C / methanol / 16 h

With hydrogen; lithium bromide; palladium on activated charcoal; In methanol; acetonitrile;
DOI:10.1002/anie.200462702