Technology Process of C30H31NOSi
There total 4 articles about C30H31NOSi which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium phosphate;
bis(tricyclohexylphosphine)nickel(II) dichloride;
In
toluene;
at 110 ℃;
for 24h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium phosphate / toluene / 80 °C
2: N-Bromosuccinimide / acetic acid / 60 °C
3: potassium phosphate / tetrakis(triphenylphosphine) palladium(0) / toluene; water / 90 °C
4: potassium phosphate / bis(tricyclohexylphosphine)nickel(II) dichloride / toluene / 24 h / 110 °C
With
potassium phosphate; N-Bromosuccinimide;
tetrakis(triphenylphosphine) palladium(0); bis(tricyclohexylphosphine)nickel(II) dichloride;
In
water; acetic acid; toluene;
4: Suzuki-Miyaura Coupling;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium phosphate / tetrakis(triphenylphosphine) palladium(0) / toluene; water / 90 °C
2: potassium phosphate / bis(tricyclohexylphosphine)nickel(II) dichloride / toluene / 24 h / 110 °C
With
potassium phosphate;
tetrakis(triphenylphosphine) palladium(0); bis(tricyclohexylphosphine)nickel(II) dichloride;
In
water; toluene;
2: Suzuki-Miyaura Coupling;