4-Pyridinecarboxylicacid,3-(2-propenylamino)-,ethylester(9CI)

Base Information Edit

Chemical Name:4-Pyridinecarboxylicacid,3-(2-propenylamino)-,ethylester(9CI)
CAS No.:157361-40-5
Molecular Formula:C11H14 N2 O2
Molecular Weight:206.24
Hs Code.:
Mol file:157361-40-5.mol

Synonyms:4-Pyridinecarboxylicacid, 3-(2-propenylamino)-, ethyl ester (9CI)

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Chemical Property of 4-Pyridinecarboxylicacid,3-(2-propenylamino)-,ethylester(9CI) Edit

Chemical Property:

PSA：51.22000
LogP:1.92920

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-Pyridinecarboxylicacid,3-(2-propenylamino)-,ethylester(9CI)

There total 3 articles about 4-Pyridinecarboxylicacid,3-(2-propenylamino)-,ethylester(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7579-20-6
3-Aminopyridine-4-carboxylic acid

: 157361-40-5
ethyl 3-allylaminopyridine-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: H₂SO₄ / 4 h / Heating

2: 1.) DMPU, lithium hexamethyl disilazide / 1.) THF, 0 deg C, 30 min, 2.) THF, RT, overnight

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; sulfuric acid; lithium hexamethyldisilazane;
DOI:10.1021/jm00070a012

Reference yield:

: 14208-83-4
ethyl 3-aminopyridine-4-carboxylate

: 106-95-6
allyl bromide

: 157361-40-5
ethyl 3-allylaminopyridine-4-carboxylate

Guidance literature:: With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; lithium hexamethyldisilazane; Yield given. Multistep reaction; 1.) THF, 0 deg C, 30 min, 2.) THF, RT, overnight;
DOI:10.1021/jm00070a012