tert-butyl 5'-(benzyloxycarbonyl)-3'-(2-chloroethyl)-4-(2-methoxycarbonylethyl)-3,4'-dimethyl-2,2'-dipyrrylmethane-5-carboxylate

Base Information

Chemical Name:tert-butyl 5'-(benzyloxycarbonyl)-3'-(2-chloroethyl)-4-(2-methoxycarbonylethyl)-3,4'-dimethyl-2,2'-dipyrrylmethane-5-carboxylate
CAS No.:51089-85-1
Molecular Formula:C₃₀H₃₇ClN₂O₆
Molecular Weight:557.087
Hs Code.:

Synonyms:tert-butyl 5'-(benzyloxycarbonyl)-3'-(2-chloroethyl)-4-(2-methoxycarbonylethyl)-3,4'-dimethyl-2,2'-dipyrrylmethane-5-carboxylate

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Chemical Property of tert-butyl 5'-(benzyloxycarbonyl)-3'-(2-chloroethyl)-4-(2-methoxycarbonylethyl)-3,4'-dimethyl-2,2'-dipyrrylmethane-5-carboxylate

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MSDS Files:: SDS file from LookChem

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Technology Process of tert-butyl 5'-(benzyloxycarbonyl)-3'-(2-chloroethyl)-4-(2-methoxycarbonylethyl)-3,4'-dimethyl-2,2'-dipyrrylmethane-5-carboxylate

There total 2 articles about tert-butyl 5'-(benzyloxycarbonyl)-3'-(2-chloroethyl)-4-(2-methoxycarbonylethyl)-3,4'-dimethyl-2,2'-dipyrrylmethane-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 42419-19-2
tert-butyl 3-(2-methoxycarbonylethyl)-4-methylpyrrole-2-carboxylate

: 37945-74-7
benzyl 5-acetoxymethyl-4-(2-chloroethyl)-3-methylpyrrole-2-carboxylate

: 51089-85-1
tert-butyl 5'-(benzyloxycarbonyl)-3'-(2-chloroethyl)-4-(2-methoxycarbonylethyl)-3,4'-dimethyl-2,2'-dipyrrylmethane-5-carboxylate

Guidance literature:: With Montmorillonite clay K-10; In chloroform; for 24h;
DOI:10.1021/jo981473f

Reference yield:

: 51089-85-1
tert-butyl 5'-(benzyloxycarbonyl)-3'-(2-chloroethyl)-4-(2-methoxycarbonylethyl)-3,4'-dimethyl-2,2'-dipyrrylmethane-5-carboxylate

Guidance literature:: Acetoxymethylpyrrol 7, 4-(2-Methoxycarbonylaethyl)-3-methyl-pyrrol-5-carbonsaeure-tert-butylester, Essigsaeure, p-Toluolsulfonsaeure;

Reference yield: 75.0%

: 18818-25-2
methyl 3-(5-formyl-2,4-dimethyl-1H-pyrrol-3-yl)propanoate

: 51089-85-1
tert-butyl 5'-(benzyloxycarbonyl)-3'-(2-chloroethyl)-4-(2-methoxycarbonylethyl)-3,4'-dimethyl-2,2'-dipyrrylmethane-5-carboxylate

: 438618-59-8
benzyl 3-(2-chloroethyl)-8,13-bis(2-methoxycarbonylethyl)-2,7,12,14-tetramethyl-5,16-dihydrotripyrrin-1-carboxylate hydrobromide

Guidance literature:: tert-butyl 5'-(benzyloxycarbonyl)-3'-(2-chloroethyl)-4-(2-methoxycarbonylethyl)-3,4'-dimethyl-2,2'-dipyrrylmethane-5-carboxylate; With trifluoroacetic acid; at 20 ℃; for 0.0833333h; Inert atmosphere;

methyl 3-(5-formyl-2,4-dimethyl-1H-pyrrol-3-yl)propanoate; In methanol; for 1.5h; Inert atmosphere;

With hydrogen bromide; In methanol; acetic acid;
DOI:10.1021/jo100083t