benzyl 3-(2-chloroethyl)-8,13-bis(2-methoxycarbonylethyl)-2,7,12,14-tetramethyl-5,16-dihydrotripyrrin-1-carboxylate hydrobromide

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Chemical Name:benzyl 3-(2-chloroethyl)-8,13-bis(2-methoxycarbonylethyl)-2,7,12,14-tetramethyl-5,16-dihydrotripyrrin-1-carboxylate hydrobromide
CAS No.:438618-59-8
Molecular Formula:BrH*C₃₆H₄₂ClN₃O₆
Molecular Weight:729.111
Hs Code.:

Synonyms:benzyl 3-(2-chloroethyl)-8,13-bis(2-methoxycarbonylethyl)-2,7,12,14-tetramethyl-5,16-dihydrotripyrrin-1-carboxylate hydrobromide

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Chemical Property of benzyl 3-(2-chloroethyl)-8,13-bis(2-methoxycarbonylethyl)-2,7,12,14-tetramethyl-5,16-dihydrotripyrrin-1-carboxylate hydrobromide

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Technology Process of benzyl 3-(2-chloroethyl)-8,13-bis(2-methoxycarbonylethyl)-2,7,12,14-tetramethyl-5,16-dihydrotripyrrin-1-carboxylate hydrobromide

There total 1 articles about benzyl 3-(2-chloroethyl)-8,13-bis(2-methoxycarbonylethyl)-2,7,12,14-tetramethyl-5,16-dihydrotripyrrin-1-carboxylate hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 18818-25-2
methyl 3-(5-formyl-2,4-dimethyl-1H-pyrrol-3-yl)propanoate

: 51089-85-1
tert-butyl 5'-(benzyloxycarbonyl)-3'-(2-chloroethyl)-4-(2-methoxycarbonylethyl)-3,4'-dimethyl-2,2'-dipyrrylmethane-5-carboxylate

: 438618-59-8
benzyl 3-(2-chloroethyl)-8,13-bis(2-methoxycarbonylethyl)-2,7,12,14-tetramethyl-5,16-dihydrotripyrrin-1-carboxylate hydrobromide

Guidance literature:: tert-butyl 5'-(benzyloxycarbonyl)-3'-(2-chloroethyl)-4-(2-methoxycarbonylethyl)-3,4'-dimethyl-2,2'-dipyrrylmethane-5-carboxylate; With trifluoroacetic acid; at 20 ℃; for 0.0833333h; Inert atmosphere;

methyl 3-(5-formyl-2,4-dimethyl-1H-pyrrol-3-yl)propanoate; In methanol; for 1.5h; Inert atmosphere;

With hydrogen bromide; In methanol; acetic acid;
DOI:10.1021/jo100083t