n-butyloxotin cyclohexanoate hexamer

Base Information

• Chemical Name: n-butyloxotin cyclohexanoate hexamer
• CAS No.: 107147-92-2
• Molecular Formula: C₆H₆*C₆₆H₁₂₀O₁₈Sn₆
• Molecular Weight: 1992.04
• Mol file: 107147-92-2.mol

Synonyms:n-butyloxotin cyclohexanoate hexamer

Chemical Property of n-butyloxotin cyclohexanoate hexamer

Chemical Property:

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Technology Process of n-butyloxotin cyclohexanoate hexamer

There total 1 articles about n-butyloxotin cyclohexanoate hexamer which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

n-butylstannoic acid (2273-43-0) + Cyclohexanecarboxylic acid (98-89-5) → n-butyloxotin cyclohexanoate hexamer (107147-92-2)

Guidance literature:

With C₆H₆; In benzene; byproducts: H2O; react. of carboxylic acid and n-butylstannanoic acid in C6H6 under reflux for 4 h (Dean-Stark apparatus); removal of C6H6 (rotary evapn.), dissoln. of solid in hot benzene, keeping in a refrigerator for crystn., drying; elem. anal.;

DOI:10.1021/ic00254a017

upstream raw materials:

n-butylstannoic acid

Cyclohexanecarboxylic acid

Refernces