[Pd₂(k2-C,S-CH(STol-p)(C₆H(STol-p-2)(OMe)3-3,4,5))(2,2'-bipyridine)I]

Base Information

Chemical Name:[Pd₂(k2-C,S-CH(STol-p)(C₆H(STol-p-2)(OMe)3-3,4,5))(2,2'-bipyridine)I]
CAS No.:334912-12-8
Molecular Formula:C₃₄H₃₃IN₂O₃PdS₂
Molecular Weight:815.104
Hs Code.:

[Pd<sub>2</sub>(k2-C,S-CH(STol-p)(C<sub>6</sub>H(STol-p-2)(OMe)3-3,4,5))(2,2'-bipyridine)I]

Synonyms:[Pd₂(k2-C,S-CH(STol-p)(C₆H(STol-p-2)(OMe)3-3,4,5))(2,2'-bipyridine)I]

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Chemical Property of [Pd₂(k2-C,S-CH(STol-p)(C₆H(STol-p-2)(OMe)3-3,4,5))(2,2'-bipyridine)I]

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Technology Process of [Pd₂(k2-C,S-CH(STol-p)(C₆H(STol-p-2)(OMe)3-3,4,5))(2,2'-bipyridine)I]

There total 4 articles about [Pd₂(k2-C,S-CH(STol-p)(C₆H(STol-p-2)(OMe)3-3,4,5))(2,2'-bipyridine)I] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 366-18-7
[2,2]bipyridinyl

: 334912-02-6
C₆H(OCH₃)3ICH(SC₆H₄CH₃)2

: 32005-36-0
bis(dibenzylideneacetone)-palladium⁽⁰⁾

: 334912-12-8
[Pd₂(k2-C,S-CH(STol-p)(C₆H(STol-p-2)(OMe)3-3,4,5))(2,2'-bipyridine)I]

Guidance literature:: In toluene; to a mixt. of complex and bipyridine in toluene was added iodoarene, themixt. was stirred at room temp. under N2 for 20 h; evapd. in vac., the residue was extd. with CH2Cl2, filtered, pptn. by adding of Et2O, filtered, washed with Et2O, air-dried;
DOI:10.1021/om0008981

Reference yield: 67.0%

: 334912-11-7
[Pd₂(k2-C,S-CH(STol-p)(C₆H(STol-p-2)(OMe)3-3,4,5))(2,2'-bipyridine)]OSO₂CF₃

: 7681-82-5,24359-64-6,41927-88-2,115813-40-6
sodium iodide

: 334912-12-8
[Pd₂(k2-C,S-CH(STol-p)(C₆H(STol-p-2)(OMe)3-3,4,5))(2,2'-bipyridine)I]

Guidance literature:: In acetone; the mixt. in acetone was stirred for 1 h; evapd., the residue was extd. with CH2Cl2, filtered, evapd., Et2O was added, ppt. was filtered, washed with Et2O and air-dried; elem. anal.;
DOI:10.1021/om0008981

Reference yield:

: 334912-05-9
[Pd2(k2-C,S-CH(STol-p)(C6H(STol-p-2)(OMe)3-3,4,5))2(μ-I)2]

: 334912-12-8
[Pd₂(k2-C,S-CH(STol-p)(C₆H(STol-p-2)(OMe)3-3,4,5))(2,2'-bipyridine)I]

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane

2: acetone

In dichloromethane; acetone;
DOI:10.1021/om0008981