tris(4-azidophenyl)amine

Base Information

Chemical Name:tris(4-azidophenyl)amine
CAS No.:1297583-31-3
Molecular Formula:C₁₈H₁₂N₁₀
Molecular Weight:368.36
Hs Code.:

Synonyms:tris(4-azidophenyl)amine

Suppliers and Price of tris(4-azidophenyl)amine

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Chemical Property of tris(4-azidophenyl)amine

Chemical Property:

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Technology Process of tris(4-azidophenyl)amine

There total 4 articles about tris(4-azidophenyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 5981-09-9
4,4',4-triaminotriphenylamine

: 1297583-31-3
tris(4-azidophenyl)amine

Guidance literature:: 4,4',4-triaminotriphenylamine; With trifluoroacetic acid; sodium nitrite; In water; at 0 ℃; for 0.25h;

With sodium azide; In water; at 0 - 20 ℃;
DOI:10.1016/j.polymer.2011.02.042

Reference yield:

: 4316-57-8
4-nitrophenyldiphenylamine

: 1297583-31-3
tris(4-azidophenyl)amine

Guidance literature:: Multi-step reaction with 2 steps

1.1: palladium on activated charcoal; hydrazine hydrate / ethanol / Reflux; Inert atmosphere

2.1: sodium nitrite; hydrogenchloride / water / Inert atmosphere

2.2: Inert atmosphere

With hydrogenchloride; palladium on activated charcoal; hydrazine hydrate; sodium nitrite; In ethanol; water;
DOI:10.1039/c7ra09558a

Reference yield:

: 603-34-9
N,N-diphenylaminobenzene

: 1297583-31-3
tris(4-azidophenyl)amine

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid; sodium nitrate / chloroform / 85 °C / Inert atmosphere

2.1: palladium on activated charcoal; hydrazine hydrate / ethanol / Reflux; Inert atmosphere

3.1: sodium nitrite; hydrogenchloride / water / Inert atmosphere

3.2: Inert atmosphere

With hydrogenchloride; sodium nitrate; palladium on activated charcoal; hydrazine hydrate; acetic acid; sodium nitrite; In ethanol; chloroform; water;
DOI:10.1039/c7ra09558a