1-<2-(benzyloxycarbonyl)-2-<(tert-butoxycarbonyl)amino>ethenyl>-2-methylnaphthalene

Base Information

Chemical Name:1-<2-(benzyloxycarbonyl)-2-<(tert-butoxycarbonyl)amino>ethenyl>-2-methylnaphthalene
CAS No.:130247-11-9
Molecular Formula:C₂₆H₂₇NO₄
Molecular Weight:417.505
Hs Code.:

Synonyms:1-<2-(benzyloxycarbonyl)-2-<(tert-butoxycarbonyl)amino>ethenyl>-2-methylnaphthalene

Suppliers and Price of 1-<2-(benzyloxycarbonyl)-2-<(tert-butoxycarbonyl)amino>ethenyl>-2-methylnaphthalene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-<2-(benzyloxycarbonyl)-2-<(tert-butoxycarbonyl)amino>ethenyl>-2-methylnaphthalene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-<2-(benzyloxycarbonyl)-2-<(tert-butoxycarbonyl)amino>ethenyl>-2-methylnaphthalene

There total 2 articles about 1-<2-(benzyloxycarbonyl)-2-<(tert-butoxycarbonyl)amino>ethenyl>-2-methylnaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 36374-82-0
1-iodo-2-methylnaphthalene

: 94882-75-4
benzyl (2-t-butoxycarbonylamino)acrylate

: 130247-11-9
1-<2-(benzyloxycarbonyl)-2-<(tert-butoxycarbonyl)amino>ethenyl>-2-methylnaphthalene

Guidance literature:: With tetrabutyl-ammonium chloride; sodium hydrogencarbonate; palladium diacetate; In N,N-dimethyl-formamide; at 85 ℃; for 16h;
DOI:10.1021/jo00003a065

Reference yield:

: 2586-62-1
1-bromo-2-methylnaphtalene

: 130247-11-9
1-<2-(benzyloxycarbonyl)-2-<(tert-butoxycarbonyl)amino>ethenyl>-2-methylnaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: 1) BuLi, 2) iodine / 1) diethyl ether, hexane, r.t., 2) diethyl ether, -70 deg C to r.t.

2: 67 percent / Bu₄NCl, NaHCO₃ / Pd(OAc)2 / dimethylformamide / 16 h / 85 °C

With n-butyllithium; tetrabutyl-ammonium chloride; iodine; sodium hydrogencarbonate; palladium diacetate; In N,N-dimethyl-formamide;
DOI:10.1021/jo00003a065