N,N'-(5,5'-(3,3'-(butane-1,4-diylbis(oxy))bis(3,1-phenylene))bis(4-acetyl-4,5-dihydro-1,3,4-thiadiazole-5,2-diyl))diacetamide

Base Information

Chemical Name:N,N'-(5,5'-(3,3'-(butane-1,4-diylbis(oxy))bis(3,1-phenylene))bis(4-acetyl-4,5-dihydro-1,3,4-thiadiazole-5,2-diyl))diacetamide
CAS No.:1401456-76-5
Molecular Formula:C₂₈H₃₂N₆O₆S₂
Molecular Weight:612.731
Hs Code.:

Synonyms:N,N'-(5,5'-(3,3'-(butane-1,4-diylbis(oxy))bis(3,1-phenylene))bis(4-acetyl-4,5-dihydro-1,3,4-thiadiazole-5,2-diyl))diacetamide

Suppliers and Price of N,N'-(5,5'-(3,3'-(butane-1,4-diylbis(oxy))bis(3,1-phenylene))bis(4-acetyl-4,5-dihydro-1,3,4-thiadiazole-5,2-diyl))diacetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N,N'-(5,5'-(3,3'-(butane-1,4-diylbis(oxy))bis(3,1-phenylene))bis(4-acetyl-4,5-dihydro-1,3,4-thiadiazole-5,2-diyl))diacetamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N,N'-(5,5'-(3,3'-(butane-1,4-diylbis(oxy))bis(3,1-phenylene))bis(4-acetyl-4,5-dihydro-1,3,4-thiadiazole-5,2-diyl))diacetamide

There total 3 articles about N,N'-(5,5'-(3,3'-(butane-1,4-diylbis(oxy))bis(3,1-phenylene))bis(4-acetyl-4,5-dihydro-1,3,4-thiadiazole-5,2-diyl))diacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1401456-62-9
2,2'-(3,3'-(butane-1,4-diylbis(oxy))bis(3,1-phenylene))bis(methan-1-yl-1-ylidene)bis(hydrazinecarbothioamide)

: 108-24-7
acetic anhydride

: 1401456-76-5
N,N'-(5,5'-(3,3'-(butane-1,4-diylbis(oxy))bis(3,1-phenylene))bis(4-acetyl-4,5-dihydro-1,3,4-thiadiazole-5,2-diyl))diacetamide

Guidance literature:: for 10h; Reflux;
DOI:10.1016/j.saa.2012.06.030

Reference yield:

: 121799-26-6
3,3'-[butane-1,3-diylbis(oxy)]dibenzaldehyde

: 1401456-76-5
N,N'-(5,5'-(3,3'-(butane-1,4-diylbis(oxy))bis(3,1-phenylene))bis(4-acetyl-4,5-dihydro-1,3,4-thiadiazole-5,2-diyl))diacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / ethanol; water / 4 h / Reflux

2: 10 h / Reflux

With hydrogenchloride; In ethanol; water;
DOI:10.1016/j.saa.2012.06.030

Reference yield:

: 100-83-4
meta-hydroxybenzaldehyde

: 1401456-76-5
N,N'-(5,5'-(3,3'-(butane-1,4-diylbis(oxy))bis(3,1-phenylene))bis(4-acetyl-4,5-dihydro-1,3,4-thiadiazole-5,2-diyl))diacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxide / ethanol; N,N-dimethyl-formamide / 4 h / Reflux

2: hydrogenchloride / ethanol; water / 4 h / Reflux

3: 10 h / Reflux

With hydrogenchloride; potassium hydroxide; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.saa.2012.06.030