2,2'-(3,3'-(butane-1,4-diylbis(oxy))bis(3,1-phenylene))bis(methan-1-yl-1-ylidene)bis(hydrazinecarbothioamide)

Base Information

• Chemical Name: 2,2'-(3,3'-(butane-1,4-diylbis(oxy))bis(3,1-phenylene))bis(methan-1-yl-1-ylidene)bis(hydrazinecarbothioamide)
• CAS No.: 1401456-62-9
• Molecular Formula: C₂₀H₂₄N₆O₂S₂
• Molecular Weight: 444.582

Synonyms:2,2'-(3,3'-(butane-1,4-diylbis(oxy))bis(3,1-phenylene))bis(methan-1-yl-1-ylidene)bis(hydrazinecarbothioamide)

Chemical Property of 2,2'-(3,3'-(butane-1,4-diylbis(oxy))bis(3,1-phenylene))bis(methan-1-yl-1-ylidene)bis(hydrazinecarbothioamide)

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Technology Process of 2,2'-(3,3'-(butane-1,4-diylbis(oxy))bis(3,1-phenylene))bis(methan-1-yl-1-ylidene)bis(hydrazinecarbothioamide)

There total 2 articles about 2,2'-(3,3'-(butane-1,4-diylbis(oxy))bis(3,1-phenylene))bis(methan-1-yl-1-ylidene)bis(hydrazinecarbothioamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

thiosemicarbazide (79-19-6) + 3,3'-[butane-1,3-diylbis(oxy)]dibenzaldehyde (121799-26-6) → 2,2'-(3,3'-(butane-1,4-diylbis(oxy))bis(3,1-phenylene))bis(methan-1-yl-1-ylidene)bis(hydrazinecarbothioamide) (1401456-62-9)

Guidance literature:

With hydrogenchloride; In ethanol; water; for 4h; Reflux;

DOI:10.1016/j.saa.2012.06.030

Reference yield:

meta-hydroxybenzaldehyde (100-83-4) → 2,2'-(3,3'-(butane-1,4-diylbis(oxy))bis(3,1-phenylene))bis(methan-1-yl-1-ylidene)bis(hydrazinecarbothioamide) (1401456-62-9)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium hydroxide / ethanol; N,N-dimethyl-formamide / 4 h / Reflux

2: hydrogenchloride / ethanol; water / 4 h / Reflux

With hydrogenchloride; potassium hydroxide; In ethanol; water; N,N-dimethyl-formamide;

DOI:10.1016/j.saa.2012.06.030

Reference yield: 73.0%

2,2'-(3,3'-(butane-1,4-diylbis(oxy))bis(3,1-phenylene))bis(methan-1-yl-1-ylidene)bis(hydrazinecarbothioamide) (1401456-62-9) + acetic anhydride (108-24-7) → N,N'-(5,5'-(3,3'-(butane-1,4-diylbis(oxy))bis(3,1-phenylene))bis(4-acetyl-4,5-dihydro-1,3,4-thiadiazole-5,2-diyl))diacetamide (1401456-76-5)

Guidance literature:

for 10h; Reflux;

DOI:10.1016/j.saa.2012.06.030

upstream raw materials:

thiosemicarbazide

3,3'-[butane-1,3-diylbis(oxy)]dibenzaldehyde

meta-hydroxybenzaldehyde

Downstream raw materials:

N,N'-(5,5'-(3,3'-(butane-1,4-diylbis(oxy))bis(3,1-phenylene))bis(4-acetyl-4,5-dihydro-1,3,4-thiadiazole-5,2-diyl))diacetamide

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