2-(5-amino-2-phenyl-2-chloro-4-cyano-2,3-dihydrofuran-3-ylidene)propanedinitrile

Base Information

• Chemical Name: 2-(5-amino-2-phenyl-2-chloro-4-cyano-2,3-dihydrofuran-3-ylidene)propanedinitrile
• CAS No.: 1307234-14-5
• Molecular Formula: C₁₄H₇ClN₄O
• Molecular Weight: 282.689
• Mol file: 1307234-14-5.mol

Synonyms:2-(5-amino-2-phenyl-2-chloro-4-cyano-2,3-dihydrofuran-3-ylidene)propanedinitrile

Chemical Property of 2-(5-amino-2-phenyl-2-chloro-4-cyano-2,3-dihydrofuran-3-ylidene)propanedinitrile

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(5-amino-2-phenyl-2-chloro-4-cyano-2,3-dihydrofuran-3-ylidene)propanedinitrile

There total 5 articles about 2-(5-amino-2-phenyl-2-chloro-4-cyano-2,3-dihydrofuran-3-ylidene)propanedinitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

ammonium 2-benzoyl-1,1,3,3-tetracyanopropenide → 2-(5-amino-2-phenyl-2-chloro-4-cyano-2,3-dihydrofuran-3-ylidene)propanedinitrile (1307234-14-5)

Guidance literature:

With hydrogenchloride; In water; at 65 - 70 ℃; for 0.333333h;

DOI:10.1134/S107042801110006X

Reference yield: 72.0%

potassium 2-benzoyl-1,1,3,3-tetracyanoprop-2-en-1-ide (1307234-10-1) → 2-(5-amino-2-phenyl-2-chloro-4-cyano-2,3-dihydrofuran-3-ylidene)propanedinitrile (1307234-14-5)

Guidance literature:

With hydrogenchloride; In water; at 80 ℃; for 0.25h;

DOI:10.1134/S1070428011030134

Reference yield: 64.0%

sodium 2-benzoyl-1,1,3,3-tetracyanoprop-2-en-1-ide (1399841-93-0) → 2-(5-amino-2-phenyl-2-chloro-4-cyano-2,3-dihydrofuran-3-ylidene)propanedinitrile (1307234-14-5)

Guidance literature:

With hydrogenchloride; In formamide; at 20 ℃; Solvent;

DOI:10.1134/S1070428014080053

upstream raw materials:

potassium 2-benzoyl-1,1,3,3-tetracyanoprop-2-en-1-ide

3-benzoylcyclopropane-1,1,2,2,-tetracarbonitrile

sodium 2-benzoyl-1,1,3,3-tetracyanoprop-2-en-1-ide