Technology Process of sodium 2-benzoyl-1,1,3,3-tetracyanoprop-2-en-1-ide
There total 3 articles about sodium 2-benzoyl-1,1,3,3-tetracyanoprop-2-en-1-ide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
3-benzoylcyclopropane-1,1,2,2,-tetracarbonitrile;
With
sodium acetate;
In
ethanol;
at 45 - 50 ℃;
With
sodium chloride;
In
ethanol;
at 5 - 10 ℃;
for 0.5h;
DOI:10.1021/acs.joc.6b01040
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: bromine / water; ethanol / 0.5 h
2.1: sodium acetate / ethanol / 45 - 50 °C
2.2: 0.5 h / 5 - 10 °C
With
bromine; sodium acetate;
In
ethanol; water;
DOI:10.1021/acs.joc.6b01040
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium bromide; sulfuric acid / dimethyl sulfoxide / 85 - 115 °C
2.1: bromine / water; ethanol / 0.5 h
3.1: sodium acetate / ethanol / 45 - 50 °C
3.2: 0.5 h / 5 - 10 °C
With
sulfuric acid; bromine; sodium acetate; sodium bromide;
In
ethanol; water; dimethyl sulfoxide;
DOI:10.1021/acs.joc.6b01040
