Zn(II)-3-bromo-17,18-dihydro-10-mesityl-18,18-dimethylporphyrin

Base Information Edit

Chemical Name:Zn(II)-3-bromo-17,18-dihydro-10-mesityl-18,18-dimethylporphyrin
CAS No.:892861-55-1
Molecular Formula:C₃₁H₂₇BrN₄Zn
Molecular Weight:600.876
Hs Code.:
Mol file:892861-55-1.mol

Synonyms:Zn(II)-3-bromo-17,18-dihydro-10-mesityl-18,18-dimethylporphyrin

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Chemical Property of Zn(II)-3-bromo-17,18-dihydro-10-mesityl-18,18-dimethylporphyrin Edit

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Technology Process of Zn(II)-3-bromo-17,18-dihydro-10-mesityl-18,18-dimethylporphyrin

There total 2 articles about Zn(II)-3-bromo-17,18-dihydro-10-mesityl-18,18-dimethylporphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 892861-52-8
8-bromo-2,3,4,5-tetrahydro-1,3,3-trimethyldipyrrin

: 892861-47-1
1-bromo-9-formyl-5-mesityldipyrromethane

: 557-34-6
zinc diacetate

: 892861-55-1
Zn(II)-3-bromo-17,18-dihydro-10-mesityl-18,18-dimethylporphyrin

Guidance literature:: 8-bromo-2,3,4,5-tetrahydro-1,3,3-trimethyldipyrrin; 1-bromo-9-formyl-5-mesityldipyrromethane; With toluene-4-sulfonic acid; In methanol; dichloromethane; at 20 ℃; for 0.666667h; Inert atmosphere;

zinc diacetate; With 2,2,6,6-tetramethyl-piperidine; silver trifluoromethanesulfonate; In acetonitrile; for 14h; Reflux;
DOI:10.1142/S1088424615500042

Reference yield:

: C₃₁H₃₈Br₂N₄

: 892861-55-1
Zn(II)-3-bromo-17,18-dihydro-10-mesityl-18,18-dimethylporphyrin

Guidance literature:: With 2,2,6,6-tetramethyl-piperidine; zinc diacetate; silver trifluoromethanesulfonate; In acetonitrile; for 14h; Heating / reflux;