(3R,6S)-6-((3E,5E,7E)-(2S,9S,11R)-2,13-Dimethoxy-3,9,11-trimethyl-12-oxo-trideca-3,5,7-trienyl)-3-methyl-tetrahydro-pyran-2-one

Base Information

Chemical Name:(3R,6S)-6-((3E,5E,7E)-(2S,9S,11R)-2,13-Dimethoxy-3,9,11-trimethyl-12-oxo-trideca-3,5,7-trienyl)-3-methyl-tetrahydro-pyran-2-one
CAS No.:146404-46-8
Molecular Formula:C₂₄H₃₈O₅
Molecular Weight:406.563
Hs Code.:

Synonyms:(3R,6S)-6-((3E,5E,7E)-(2S,9S,11R)-2,13-Dimethoxy-3,9,11-trimethyl-12-oxo-trideca-3,5,7-trienyl)-3-methyl-tetrahydro-pyran-2-one

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Chemical Property of (3R,6S)-6-((3E,5E,7E)-(2S,9S,11R)-2,13-Dimethoxy-3,9,11-trimethyl-12-oxo-trideca-3,5,7-trienyl)-3-methyl-tetrahydro-pyran-2-one

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Technology Process of (3R,6S)-6-((3E,5E,7E)-(2S,9S,11R)-2,13-Dimethoxy-3,9,11-trimethyl-12-oxo-trideca-3,5,7-trienyl)-3-methyl-tetrahydro-pyran-2-one

There total 6 articles about (3R,6S)-6-((3E,5E,7E)-(2S,9S,11R)-2,13-Dimethoxy-3,9,11-trimethyl-12-oxo-trideca-3,5,7-trienyl)-3-methyl-tetrahydro-pyran-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1156545-82-2
C₆₀H₁₀₃NO₁₃Si

: 1156545-83-3
C₃₆H₆₅NO₈Si

: 146404-46-8
(3R,6S)-6-((3E,5E,7E)-(2S,9S,11R)-2,13-Dimethoxy-3,9,11-trimethyl-12-oxo-trideca-3,5,7-trienyl)-3-methyl-tetrahydro-pyran-2-one

Guidance literature:: With zinc(II) chloride; In tetrahydrofuran; diethyl ether; at 20 - 60 ℃; for 1h; Inert atmosphere;
DOI:10.1002/chem.200801656

Reference yield:

: 146404-44-6
C₅₂H₈₁NO₁₄

: 146404-46-8
(3R,6S)-6-((3E,5E,7E)-(2S,9S,11R)-2,13-Dimethoxy-3,9,11-trimethyl-12-oxo-trideca-3,5,7-trienyl)-3-methyl-tetrahydro-pyran-2-one

: 146404-45-7
(2E,6E)-(4R,8R)-9-((1S,3R,4R)-4-Hydroxy-3-methoxy-cyclohexyl)-2,4,8-trimethyl-5-oxo-nona-2,6-dienal

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; at -78 - -20 ℃; Yield given. Yields of byproduct given;
DOI:10.1016/S0040-4039(00)60797-9

Reference yield:

: 146404-52-6
C₆₁H₁₀₃NO₁₄Si

: 146404-46-8
(3R,6S)-6-((3E,5E,7E)-(2S,9S,11R)-2,13-Dimethoxy-3,9,11-trimethyl-12-oxo-trideca-3,5,7-trienyl)-3-methyl-tetrahydro-pyran-2-one

: 146404-54-8
(S)-1-Methoxyoxalyl-piperidine-2-carboxylic acid (E)-(1S,4R)-3-hydroxy-1-[(R)-2-((1S,3R,4R)-3-methoxy-4-triisopropylsilanyloxy-cyclohexyl)-1-methyl-ethyl]-4,6-dimethyl-7-oxo-hept-5-enyl ester

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; at -78 - -20 ℃; Yield given. Yields of byproduct given;
DOI:10.1016/S0040-4039(00)60797-9