C₂₇H₂₂N₂O₄S

Base Information

Chemical Name:C₂₇H₂₂N₂O₄S
CAS No.:1423685-07-7
Molecular Formula:C₂₇H₂₂N₂O₄S
Molecular Weight:470.549
Hs Code.:

C<sub>27</sub>H<sub>22</sub>N<sub>2</sub>O<sub>4</sub>S

Synonyms:C₂₇H₂₂N₂O₄S

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Chemical Property of C₂₇H₂₂N₂O₄S

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Technology Process of C₂₇H₂₂N₂O₄S

There total 9 articles about C₂₇H₂₂N₂O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.5%

: 1423691-32-0
C₂₈H₂₄N₂O₄S

: 1423685-07-7
C₂₇H₂₂N₂O₄S

Guidance literature:: C₂₈H₂₄N₂O₄S; With lithium hydroxide monohydrate; water; In tetrahydrofuran; at 20 ℃;

With hydrogenchloride; In water; pH=2;

Reference yield:

: 33626-98-1
methyl 6-bromo-2-naphthoate

: 1423685-07-7
C₂₇H₂₂N₂O₄S

Guidance literature:: Multi-step reaction with 9 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.5 h / 0 - 20 °C

2.1: thionyl chloride; zinc(II) chloride / dichloromethane / -5 - 20 °C

3.1: acetonitrile / Reflux

4.1: acetic acid; water; sulfuric acid / 2 h / Reflux

5.1: hydrogenchloride / 2 h / Reflux

6.1: triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide / N,N-dimethyl-formamide / Inert atmosphere; Reflux

7.1: tetrabutyl ammonium fluoride / dichloromethane / 2 h / 20 °C

8.1: triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide / 2 h / Inert atmosphere; Reflux

9.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 20 °C

9.2: pH 2

With hydrogenchloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide; lithium aluminium tetrahydride; thionyl chloride; lithium hydroxide monohydrate; sulfuric acid; tetrabutyl ammonium fluoride; water; acetic acid; triethylamine; zinc(II) chloride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 305798-03-2
2-(6-bromonaphthalen-2-yl)acetonitrile

: 1423685-07-7
C₂₇H₂₂N₂O₄S

Guidance literature:: Multi-step reaction with 6 steps

1.1: acetic acid; water; sulfuric acid / 2 h / Reflux

2.1: hydrogenchloride / 2 h / Reflux

3.1: triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide / N,N-dimethyl-formamide / Inert atmosphere; Reflux

4.1: tetrabutyl ammonium fluoride / dichloromethane / 2 h / 20 °C

5.1: triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide / 2 h / Inert atmosphere; Reflux

6.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 20 °C

6.2: pH 2

With hydrogenchloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide; lithium hydroxide monohydrate; sulfuric acid; tetrabutyl ammonium fluoride; water; acetic acid; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;