(S)-di-tert-butyl (6-((3,5-bis(phenylethynyl) phenyl)amino)-6-oxohexane-1,5-diyl)dicarbamate

Base Information

Chemical Name:(S)-di-tert-butyl (6-((3,5-bis(phenylethynyl) phenyl)amino)-6-oxohexane-1,5-diyl)dicarbamate
CAS No.:1412499-33-2
Molecular Formula:C₃₈H₄₃N₃O₅
Molecular Weight:621.777
Hs Code.:

Synonyms:(S)-di-tert-butyl (6-((3,5-bis(phenylethynyl) phenyl)amino)-6-oxohexane-1,5-diyl)dicarbamate

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Chemical Property of (S)-di-tert-butyl (6-((3,5-bis(phenylethynyl) phenyl)amino)-6-oxohexane-1,5-diyl)dicarbamate

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Technology Process of (S)-di-tert-butyl (6-((3,5-bis(phenylethynyl) phenyl)amino)-6-oxohexane-1,5-diyl)dicarbamate

There total 2 articles about (S)-di-tert-butyl (6-((3,5-bis(phenylethynyl) phenyl)amino)-6-oxohexane-1,5-diyl)dicarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 900518-37-8
3,5-bis(phenylethynyl)aniline

: 2483-46-7
Boc-Lys(Boc)-OH

: 1412499-33-2
(S)-di-tert-butyl (6-((3,5-bis(phenylethynyl) phenyl)amino)-6-oxohexane-1,5-diyl)dicarbamate

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 - 20 ℃; for 18.5h;

Reference yield:

: 867017-50-3
((5-nitro-1,3-phenylene)bis(ethyne-2,1-diyl))dibenzene

: 1412499-33-2
(S)-di-tert-butyl (6-((3,5-bis(phenylethynyl) phenyl)amino)-6-oxohexane-1,5-diyl)dicarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; tin(ll) chloride / water; tetrahydrofuran / 3 h / 20 °C

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 18.5 h / 0 - 20 °C

With hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; tin(ll) chloride; In tetrahydrofuran; dichloromethane; water;