3,4-Dihydroxy-2-(3-methylbut-2-enyl)benzaldehyde

Base Information

• Chemical Name: 3,4-Dihydroxy-2-(3-methylbut-2-enyl)benzaldehyde
• CAS No.: 157027-24-2
• Molecular Formula: C12H14 O3
• Molecular Weight: 206.23776
• DSSTox Substance ID: DTXSID70447241
• Mol file: 157027-24-2.mol

Synonyms:157027-24-2;3,4-dihydroxy-2-(3-methylbut-2-enyl)benzaldehyde;Benzaldehyde, 3,4-dihydroxy-2-(3-methyl-2-butenyl)- (9CI);3,4-Dihydroxy-2-(3-methyl-2-buten-1-yl)benzaldehyde;SCHEMBL4263088;DTXSID70447241;3,4-Dihydroxy-2-(3-methylbut-2-en-1-yl)benzaldehyde;Benzaldehyde,3,4-dihydroxy-2-(3-methyl-2-butenyl)-(9ci)

Chemical Property of 3,4-Dihydroxy-2-(3-methylbut-2-enyl)benzaldehyde

Chemical Property:

• Boiling Point: 351.8±37.0 °C(Predicted)
• PKA: 7.67±0.23(Predicted)
• PSA: 57.53000
• Density: 1.187±0.06 g/cm3(Predicted)
• LogP: 2.41900
• XLogP3: 2.6
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 206.094294304
• Heavy Atom Count: 15
• Complexity: 243

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=CCC1=C(C=CC(=C1O)O)C=O)C

Technology Process of 3,4-Dihydroxy-2-(3-methylbut-2-enyl)benzaldehyde

There total 1 articles about 3,4-Dihydroxy-2-(3-methylbut-2-enyl)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

prenyl bromide (870-63-3) + 3,4-dihydroxybenzaldehyde (139-85-5) → 3,4-Dihydroxy-2-(3-methyl-but-2-enyl)-benzaldehyde (157027-24-2)

Guidance literature:

With potassium hydroxide; In water; for 24h; Ambient temperature;

DOI:10.1080/00304949609356517

Reference yield: 92.0%

dimethyl sulfate (77-78-1) + 3,4-Dihydroxy-2-(3-methyl-but-2-enyl)-benzaldehyde (157027-24-2) → 3,4-Dimethoxy-2-(3-methyl-but-2-enyl)-benzaldehyde (157027-25-3)

Guidance literature:

With potassium carbonate; In acetone; for 3h; Heating;

DOI:10.1080/00304949609356517

Reference yield: 85.0%

chloromethyl methyl ether (107-30-2) + 3,4-Dihydroxy-2-(3-methyl-but-2-enyl)-benzaldehyde (157027-24-2) → 3,4-bis(methoxymethoxy)-2-(3-methylbut-2-enyl)benzaldehyde (495412-07-2)

Guidance literature:

With potassium carbonate; In acetone; for 0.5h; Heating;

DOI:10.1080/00304949609356517

upstream raw materials:

prenyl bromide

3,4-dihydroxybenzaldehyde

Downstream raw materials:

3,4-bis(methoxymethoxy)-2-(3-methylbut-2-enyl)benzaldehyde

3,4-Dimethoxy-2-(3-methyl-but-2-enyl)-benzaldehyde

antiarone F

3,4-Bis-methoxymethoxy-2,5-bis-(3-methyl-but-2-enyl)-benzaldehyde