C₃₄H₃₁O₃P

Base Information

Chemical Name:C₃₄H₃₁O₃P
CAS No.:1579997-30-0
Molecular Formula:C₃₄H₃₁O₃P
Molecular Weight:518.592
Hs Code.:

C<sub>34</sub>H<sub>31</sub>O<sub>3</sub>P

Synonyms:C₃₄H₃₁O₃P

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Chemical Property of C₃₄H₃₁O₃P

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Technology Process of C₃₄H₃₁O₃P

There total 5 articles about C₃₄H₃₁O₃P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1579997-16-2
C₃₃H₂₉O₃P

: 74-88-4
methyl iodide

: 1579997-30-0
C₃₄H₃₁O₃P

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 12h; Inert atmosphere; Schlenk technique;
DOI:10.1021/ja501007t

Reference yield:

: 644-97-3
Dichlorophenylphosphine

: 1579997-30-0
C₃₄H₃₁O₃P

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran / 4 h / -80 - 20 °C / Inert atmosphere; Schlenk technique

1.2: 2 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

2.1: C₁₈H₂₂N₃Pd⁽¹⁺⁾*ClO₄^(1-) / chloroform / 0.03 h / 20 °C / Inert atmosphere; Schlenk technique

2.2: 10 h / -45 °C / Inert atmosphere; Schlenk technique

2.3: 8 h / -45 °C / Inert atmosphere; Schlenk technique

3.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere; Schlenk technique

With C₁₈H₂₂N₃Pd⁽¹⁺⁾*ClO₄^(1-); potassium carbonate; In tetrahydrofuran; chloroform; N,N-dimethyl-formamide;
DOI:10.1021/ja501007t

Reference yield:

: 2633-66-1
2-mesitylmagnesium bromide

: 1579997-30-0
C₃₄H₃₁O₃P

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran / 4 h / -80 - 20 °C / Inert atmosphere; Schlenk technique

1.2: 2 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

2.1: C₁₈H₂₂N₃Pd⁽¹⁺⁾*ClO₄^(1-) / chloroform / 0.03 h / 20 °C / Inert atmosphere; Schlenk technique

2.2: 10 h / -45 °C / Inert atmosphere; Schlenk technique

2.3: 8 h / -45 °C / Inert atmosphere; Schlenk technique

3.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere; Schlenk technique

With C₁₈H₂₂N₃Pd⁽¹⁺⁾*ClO₄^(1-); potassium carbonate; In tetrahydrofuran; chloroform; N,N-dimethyl-formamide;
DOI:10.1021/ja501007t