2-naphthylmethyl O-(methyl 2,3-di-O-benzoyl-4-O-levulinoyl-β-D-glucopyranosyluronate)-(1->3)-4,6-di-O-benzoyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside

Base Information

• Chemical Name: 2-naphthylmethyl O-(methyl 2,3-di-O-benzoyl-4-O-levulinoyl-β-D-glucopyranosyluronate)-(1->3)-4,6-di-O-benzoyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside
• CAS No.: 1196070-76-4
• Molecular Formula: C₅₉H₅₂Cl₃NO₁₈
• Molecular Weight: 1169.42

Synonyms:2-naphthylmethyl O-(methyl 2,3-di-O-benzoyl-4-O-levulinoyl-β-D-glucopyranosyluronate)-(1->3)-4,6-di-O-benzoyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside

Chemical Property of 2-naphthylmethyl O-(methyl 2,3-di-O-benzoyl-4-O-levulinoyl-β-D-glucopyranosyluronate)-(1->3)-4,6-di-O-benzoyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside

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Technology Process of 2-naphthylmethyl O-(methyl 2,3-di-O-benzoyl-4-O-levulinoyl-β-D-glucopyranosyluronate)-(1->3)-4,6-di-O-benzoyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside

There total 1 articles about 2-naphthylmethyl O-(methyl 2,3-di-O-benzoyl-4-O-levulinoyl-β-D-glucopyranosyluronate)-(1->3)-4,6-di-O-benzoyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2S,3S,4R,5R,6R)-4,5-Dihydroxy-6-[(2R,3R,4R,5R,6R)-3-hydroxy-2-hydroxymethyl-6-(naphthalen-2-ylmethoxy)-5-(2,2,2-trichloro-acetylamino)-tetrahydro-pyran-4-yloxy]-3-(4-oxo-pentanoyloxy)-tetrahydro-pyran-2-carboxylic acid methyl ester + benzoyl chloride (98-88-4) → 2-naphthylmethyl O-(methyl 2,3-di-O-benzoyl-4-O-levulinoyl-β-D-glucopyranosyluronate)-(1->3)-4,6-di-O-benzoyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside (1196070-76-4)

Guidance literature:

With pyridine; at 0 ℃; for 2h;

DOI:10.1002/chem.200900740

Reference yield: 89.0%

2-naphthylmethyl O-(methyl 2,3-di-O-benzoyl-4-O-levulinoyl-β-D-glucopyranosyluronate)-(1->3)-4,6-di-O-benzoyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside (1196070-76-4) → 2-naphthylmethyl O-(methyl 2,3-di-O-benzoyl-β-D-glucopyranosyluronate)-(1->3)-4,6-di-O-benzoyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside (1196070-77-5)

Guidance literature:

With pyridine; hydrazine hydrate; acetic acid; at 20 ℃; for 0.133333h;

DOI:10.1002/chem.200900740

upstream raw materials:

benzoyl chloride

Downstream raw materials:

2-naphthylmethyl O-(methyl 2,3-di-O-benzoyl-β-D-glucopyranosyluronate)-(1->3)-4,6-di-O-benzoyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside

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