pentaerythrite-(tert-butyl-dimethylsilylether)-tris(para-tolylsulfonate)

Base Information

Chemical Name:pentaerythrite-(tert-butyl-dimethylsilylether)-tris(para-tolylsulfonate)
CAS No.:934964-49-5
Molecular Formula:C₃₂H₄₄O₁₀S₃Si
Molecular Weight:712.979
Hs Code.:

Synonyms:pentaerythrite-(tert-butyl-dimethylsilylether)-tris(para-tolylsulfonate)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of pentaerythrite-(tert-butyl-dimethylsilylether)-tris(para-tolylsulfonate)

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Technology Process of pentaerythrite-(tert-butyl-dimethylsilylether)-tris(para-tolylsulfonate)

There total 3 articles about pentaerythrite-(tert-butyl-dimethylsilylether)-tris(para-tolylsulfonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 244181-52-0
2-(hydroxymethyl)-2-((tosyloxy)methyl)propanyl-1,3-bis(4'-methylbenzolsulfonate)

: 18162-48-6
tert-butyldimethylsilyl chloride

: 934964-49-5
pentaerythrite-(tert-butyl-dimethylsilylether)-tris(para-tolylsulfonate)

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 24h;
DOI:10.1039/b606510b

Reference yield:

: 115-77-5
Pentaerythritol

: 934964-49-5
pentaerythrite-(tert-butyl-dimethylsilylether)-tris(para-tolylsulfonate)

Guidance literature:: Multi-step reaction with 2 steps

1: 43 percent / pyridine / 20 °C

2: 81 percent / imidazole / dimethylformamide / 24 h / 20 °C

With pyridine; 1H-imidazole; In N,N-dimethyl-formamide;
DOI:10.1039/b606510b

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 934964-49-5
pentaerythrite-(tert-butyl-dimethylsilylether)-tris(para-tolylsulfonate)

Guidance literature:: Multi-step reaction with 2 steps

1: 43 percent / pyridine / 20 °C

2: 81 percent / imidazole / dimethylformamide / 24 h / 20 °C

With pyridine; 1H-imidazole; In N,N-dimethyl-formamide;
DOI:10.1039/b606510b