α-deuterio-cyclohexanecarboxaldehyde

Base Information

Chemical Name:α-deuterio-cyclohexanecarboxaldehyde
CAS No.:62102-73-2
Molecular Formula:C₇H₁₂O
Molecular Weight:113.164
Hs Code.:

Synonyms:α-deuterio-cyclohexanecarboxaldehyde

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of α-deuterio-cyclohexanecarboxaldehyde

Chemical Property:

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Technology Process of α-deuterio-cyclohexanecarboxaldehyde

There total 6 articles about α-deuterio-cyclohexanecarboxaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 80783-98-8
N-methoxy-N-methylcyclohexanecarboxamide

: 62102-73-2
α-deuterio-cyclohexanecarboxaldehyde

Guidance literature:: With bis(η5-cyclopentadienyl)chlorozirconium deuteride; In tetrahydrofuran; at 20 ℃; for 0.166667h;
DOI:10.1016/j.tetlet.2004.02.030 DOI:10.1021/ja066362+

Reference yield: 25.0%

: 467238-80-8
cyclohexane-1,1-[2H,2H]-methanol

: 62102-73-2
α-deuterio-cyclohexanecarboxaldehyde

Guidance literature:: With dipyridinium dichromate; In various solvent(s); for 16h;
DOI:10.1021/ja027061c

Reference yield:

: 4630-82-4
methyl cyclohexylcarboxylate

: 62102-73-2
α-deuterio-cyclohexanecarboxaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: LiAlD₄ / tetrahydrofuran / 2 h / Heating

1.2: 98 percent / H₂O; NaOH / 0 °C

2.1: 25 percent / PDC / various solvent(s) / 16 h

With dipyridinium dichromate; lithium aluminium deuteride; In tetrahydrofuran;
DOI:10.1021/ja027061c