Technology Process of C36H23BrN2
There total 5 articles about C36H23BrN2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
water; toluene;
at 80 ℃;
for 6h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: iodine; acetic acid; periodic acid / 2 h / 80 °C / Inert atmosphere
2: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 6 h / 90 °C / Inert atmosphere
3: potassium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; water / 6 h / 80 °C
With
iodine; potassium acetate; potassium carbonate; acetic acid; periodic acid;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium(0);
In
water; dimethyl sulfoxide; toluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate; copper; 18-crown-6 ether / 1,2-dichloro-benzene / 48 h / 170 - 180 °C
2: iodine; acetic acid; periodic acid / 2 h / 80 °C / Inert atmosphere
3: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 6 h / 90 °C / Inert atmosphere
4: potassium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; water / 6 h / 80 °C
With
18-crown-6 ether; iodine; potassium acetate; copper; potassium carbonate; acetic acid; periodic acid;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium(0);
In
water; dimethyl sulfoxide; 1,2-dichloro-benzene; toluene;